3-Pyridinemethanol,alpha,6-dimethyl-,(-)-(9CI)

Base Information Edit

Chemical Name:3-Pyridinemethanol,alpha,6-dimethyl-,(-)-(9CI)
CAS No.:110338-86-8
Molecular Formula:C₈H₁₁NO
Molecular Weight:137.181
Hs Code.:
Mol file:110338-86-8.mol

Synonyms:3-Pyridinemethanol,alpha,6-dimethyl-,(-)-(9CI)

Suppliers and Price of 3-Pyridinemethanol,alpha,6-dimethyl-,(-)-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Pyridinemethanol,alpha,6-dimethyl-,(-)-(9CI) Edit

Chemical Property:

Purity/Quality:: 99%min ^*data from raw suppliers

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Technology Process of 3-Pyridinemethanol,alpha,6-dimethyl-,(-)-(9CI)

There total 8 articles about 3-Pyridinemethanol,alpha,6-dimethyl-,(-)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 36357-38-7
1-(6-methyl-pyridin-3-yl)-ethanone

: 56019-64-8,100189-16-0,110338-86-8
5-(1-hydroxyethyl)-2-methylpyridine

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 ℃; for 1.5h;
DOI:10.1021/jm9605694

Reference yield:

: 140-76-1,25038-86-2
2-methyl-5-vinylpyridine

: 104-90-5
5-ethyl-2-methyl-pyridine

: 56019-64-8,100189-16-0,110338-86-8
5-(1-hydroxyethyl)-2-methylpyridine

: 100189-17-1
2-(6-methylpyridin-3-yl) ethan-1-ol

Guidance literature:: With sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide; Product distribution; 1.) THF, 65 deg C, 9 h; other vinyl and propenyl heterocycles; other pyridine-BF₃ complexes; other hydroborating agents; var. temp. and time;
DOI:10.1021/jo00354a004

Reference yield:

: 2-methyl-N-[(E)-(6-methylpyridin-3-yl)methylidene]propane-2-sulfinamide

: 75-16-1
methylmagnesium bromide

: 544-97-8
dimethyl zinc(II)

: 56019-64-8,100189-16-0,110338-86-8
5-(1-hydroxyethyl)-2-methylpyridine

: 2-methyl-N-[1-(6-methylpyridin-3-yl)ethyl]propane-2-sulfinamide

Guidance literature:: methylmagnesium bromide; dimethyl zinc(II); In diethyl ether; toluene; at 15 ℃; for 0.5h; Inert atmosphere;

2-methyl-N-[(E)-(6-methylpyridin-3-yl)methylidene]propane-2-sulfinamide; In tetrahydrofuran; diethyl ether; toluene; at -78 - -70 ℃; for 1.5h; Inert atmosphere;