1-Phenyl-4-((3-(triethylsilanyl)prop-2-ynyloxy)methyl)-N,N-dimethylcyclohexanamine

Base Information

• Chemical Name: 1-Phenyl-4-((3-(triethylsilanyl)prop-2-ynyloxy)methyl)-N,N-dimethylcyclohexanamine
• CAS No.: 1184953-87-4
• Molecular Formula: C₂₄H₃₉NOSi
• Molecular Weight: 385.665

Synonyms:1-Phenyl-4-((3-(triethylsilanyl)prop-2-ynyloxy)methyl)-N,N-dimethylcyclohexanamine

Chemical Property of 1-Phenyl-4-((3-(triethylsilanyl)prop-2-ynyloxy)methyl)-N,N-dimethylcyclohexanamine

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Technology Process of 1-Phenyl-4-((3-(triethylsilanyl)prop-2-ynyloxy)methyl)-N,N-dimethylcyclohexanamine

There total 2 articles about 1-Phenyl-4-((3-(triethylsilanyl)prop-2-ynyloxy)methyl)-N,N-dimethylcyclohexanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

1-(Dimethylamino)-4-((3-(triethylsilyl)prop-2-ynyloxy)methyl)cyclohexane carbonitrile (1184953-50-1) + phenylmagnesium chloride (100-59-4) → 1-Phenyl-4-((3-(triethylsilanyl)prop-2-ynyloxy)methyl)-N,N-dimethylcyclohexanamine (1184953-87-4)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃; Product distribution / selectivity;

Reference yield: 28.0%

1-Dimethylamino-1-[1,2,3]triazol-1-yl-4-(3-triethylsilanylprop-2-ynyloxymethyl)cyclohexane (1184953-86-3) + phenylmagnesium chloride (100-59-4) → 1-Phenyl-4-((3-(triethylsilanyl)prop-2-ynyloxy)methyl)-N,N-dimethylcyclohexanamine (1184953-87-4)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃; Product distribution / selectivity;

Reference yield: 85.0%

2-iodo-4-(trifluoromethoxy)aniline (845866-79-7) + 1-Phenyl-4-((3-(triethylsilanyl)prop-2-ynyloxy)methyl)-N,N-dimethylcyclohexanamine (1184953-87-4) → N,N-Dimethyl-1-phenyl-4-(((2-(triethylsilyl)-5-(trifluoromethoxy)-1H-indol-3-yl)methoxy)methyl)cyclohexanamine (1184953-44-3)

Guidance literature:

With sodium carbonate; PEPPSI-I; In N,N-dimethyl-formamide; at 100 ℃; for 18h;

upstream raw materials:

1-(Dimethylamino)-4-((3-(triethylsilyl)prop-2-ynyloxy)methyl)cyclohexane carbonitrile

phenylmagnesium chloride

1-Dimethylamino-1-[1,2,3]triazol-1-yl-4-(3-triethylsilanylprop-2-ynyloxymethyl)cyclohexane

Downstream raw materials:

[1-phenyl-4-(2-triethylsilanyl-1H-indol-3-ylmethoxymethyl)cyclohexyl]dimethylamine

1-Phenyl-4-(((5-trifluoromethyl-2-(triethylsilyl)-1H-indol-3-yl)methoxy)methyl)-N,N-dimethylcyclohexanamine

1-(3-(((4-(Dimethylamino)-4-phenylcyclohexyl)methoxy)methyl)-5-fluoro-2-(triethylsilyl)-1H-indol-1-yl)ethanone

1-Phenyl-N,N-dimethyl-4-(((2-(triethylsilyl)-1H-pyrrolo[2,3-b]pyridin-3-yl)methoxy)methyl)cyclohexanamine

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