tricyclohexylphosphine(trimethylsilyl)borane

Base Information

Chemical Name:tricyclohexylphosphine(trimethylsilyl)borane
CAS No.:150486-99-0
Molecular Formula:C₂₁H₄₄BPSi
Molecular Weight:366.451
Hs Code.:

Synonyms:tricyclohexylphosphine(trimethylsilyl)borane

Suppliers and Price of tricyclohexylphosphine(trimethylsilyl)borane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tricyclohexylphosphine(trimethylsilyl)borane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tricyclohexylphosphine(trimethylsilyl)borane

There total 4 articles about tricyclohexylphosphine(trimethylsilyl)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 75-77-4
chloro-trimethyl-silane

: {(C₆H₁₁)3P}*BH₂Li

: 150486-99-0
tricyclohexylphosphine(trimethylsilyl)borane

Guidance literature:: In tetrahydrofuran; byproducts: LiCl; under N2 or Ar; react. Me3SiCl with (Cy)3P*BH2Li (prepared in situ from (Cy)3P*BH2I, Li powder, di-t-butyl-biphenyl and N,N,N'N'-tetramethyl-ethylenediamine in THF at 78°C) in THF at 0°C, 1 h; addn. water, extd. (Et2O, twice), extract washed (satd. aq. NaHCO3), dried (Na2SO4), concd. (vac.), soln. cooled (-25°C, crystn.);
DOI:10.1016/0022-328X(93)83347-X

Reference yield:

: 2622-14-2
tricyclohexylphosphine

: 150486-99-0
tricyclohexylphosphine(trimethylsilyl)borane

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran

2: I₂ / benzene

3: lithium-di-tert-butyl-biphenyl / tetrahydrofuran

4: tetrahydrofuran

With I₂; lithium-di-tert-butyl-biphenyl; In tetrahydrofuran; benzene;
DOI:10.1016/0022-328X(93)83347-X

Reference yield:

: PCy₃*BH₃

: 150486-99-0
tricyclohexylphosphine(trimethylsilyl)borane

Guidance literature:: Multi-step reaction with 3 steps

1: I₂ / benzene

2: lithium-di-tert-butyl-biphenyl / tetrahydrofuran

3: tetrahydrofuran

With I₂; lithium-di-tert-butyl-biphenyl; In tetrahydrofuran; benzene;
DOI:10.1016/0022-328X(93)83347-X