5-tert-butyl-N,N'-bis-[3-[2-[2-[(2-nicotinoyloxy)ethoxy]ethoxy]ethoxy]phenyl]-1,3-benzenediamide

Base Information

• Chemical Name: 5-tert-butyl-N,N'-bis-[3-[2-[2-[(2-nicotinoyloxy)ethoxy]ethoxy]ethoxy]phenyl]-1,3-benzenediamide
• CAS No.: 835874-99-2
• Molecular Formula: C₄₈H₅₄N₄O₁₂
• Molecular Weight: 878.976

Synonyms:5-tert-butyl-N,N'-bis-[3-[2-[2-[(2-nicotinoyloxy)ethoxy]ethoxy]ethoxy]phenyl]-1,3-benzenediamide

Chemical Property of 5-tert-butyl-N,N'-bis-[3-[2-[2-[(2-nicotinoyloxy)ethoxy]ethoxy]ethoxy]phenyl]-1,3-benzenediamide

Chemical Property:

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Technology Process of 5-tert-butyl-N,N'-bis-[3-[2-[2-[(2-nicotinoyloxy)ethoxy]ethoxy]ethoxy]phenyl]-1,3-benzenediamide

There total 5 articles about 5-tert-butyl-N,N'-bis-[3-[2-[2-[(2-nicotinoyloxy)ethoxy]ethoxy]ethoxy]phenyl]-1,3-benzenediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

5-tert-butyl-N,N'-bis-[3-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}phenyl]-1,3-benzenediamide (835875-15-5) + nicotinic acid (59-67-6) → 5-tert-butyl-N,N'-bis-[3-[2-[2-[(2-nicotinoyloxy)ethoxy]ethoxy]ethoxy]phenyl]-1,3-benzenediamide (835874-99-2)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 96h;

DOI:10.1039/b411583j

Reference yield:

5-tert-butyl-N,N'-bis(3-hydroxyphenyl)-1,3-benzenediamide (835875-06-4) → 5-tert-butyl-N,N'-bis-[3-[2-[2-[(2-nicotinoyloxy)ethoxy]ethoxy]ethoxy]phenyl]-1,3-benzenediamide (835874-99-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / K₂CO₃ / acetonitrile / 120 h / Heating

2: 57 percent / N-hydroxybenzotriazole,; 1-[(3-dimethylamino)propyl]-3-ethylcarbodiimide * HCl; triethylamine / CH₂Cl₂ / 96 h / 20 °C

With potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; acetonitrile;

DOI:10.1039/b411583j

Reference yield:

2-[2-(chloroethoxy)ethoxy]ethanol (5197-62-6) → 5-tert-butyl-N,N'-bis-[3-[2-[2-[(2-nicotinoyloxy)ethoxy]ethoxy]ethoxy]phenyl]-1,3-benzenediamide (835874-99-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / K₂CO₃ / acetonitrile / 120 h / Heating

2: 57 percent / N-hydroxybenzotriazole,; 1-[(3-dimethylamino)propyl]-3-ethylcarbodiimide * HCl; triethylamine / CH₂Cl₂ / 96 h / 20 °C

With potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; acetonitrile;

DOI:10.1039/b411583j

upstream raw materials:

5-tert-butyl-N,N'-bis-[3-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}phenyl]-1,3-benzenediamide

nicotinic acid

5-tert-butyl-N,N'-bis(3-hydroxyphenyl)-1,3-benzenediamide

2-[2-(chloroethoxy)ethoxy]ethanol

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