(S)-1-((1R,Z)-2-[(S)-N-methyl-S-phenylsulfonimidoyl]cyclohexyl)pent-4-en-1-ol

Base Information

Chemical Name:(S)-1-((1R,Z)-2-[(S)-N-methyl-S-phenylsulfonimidoyl]cyclohexyl)pent-4-en-1-ol
CAS No.:1380215-41-7
Molecular Formula:C₁₉H₂₇NO₂S
Molecular Weight:333.495
Hs Code.:

Synonyms:(S)-1-((1R,Z)-2-[(S)-N-methyl-S-phenylsulfonimidoyl]cyclohexyl)pent-4-en-1-ol

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Chemical Property of (S)-1-((1R,Z)-2-[(S)-N-methyl-S-phenylsulfonimidoyl]cyclohexyl)pent-4-en-1-ol

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Technology Process of (S)-1-((1R,Z)-2-[(S)-N-methyl-S-phenylsulfonimidoyl]cyclohexyl)pent-4-en-1-ol

There total 1 articles about (S)-1-((1R,Z)-2-[(S)-N-methyl-S-phenylsulfonimidoyl]cyclohexyl)pent-4-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 2100-17-6
4-pentenal

: 167389-29-9
(S)-N-methyl-S-(1-cyclohexen-1-ylmethyl)-S-phenylsulfoximine

: 1-(-2-[(S)-N-methyl-S-phenylsulfonimidoyl]cyclohexyl)pent-4-en-1-ol

: 1380215-41-7
(S)-1-((1R,Z)-2-[(S)-N-methyl-S-phenylsulfonimidoyl]cyclohexyl)pent-4-en-1-ol

Guidance literature:: (S)-N-methyl-S-(1-cyclohexen-1-ylmethyl)-S-phenylsulfoximine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

With triisopropoxytitanium(IV) chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2h; Inert atmosphere;

4-pentenal; In tetrahydrofuran; hexane; at -78 ℃; for 2.75h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1002/chem.201103060

Reference yield: 93.0%

: 994-30-9
triethylsilyl chloride

: 1380215-41-7
(S)-1-((1R,Z)-2-[(S)-N-methyl-S-phenylsulfonimidoyl]cyclohexyl)pent-4-en-1-ol

: 1380215-42-8
triethyl((S)-1-(((1R,Z)-2-[(S)-N-methyl-S-phenylsulfonimidoyl]methylene)cyclohexyl)-pent-4-enyloxy)silane

Guidance literature:: (S)-1-((1R,Z)-2-[(S)-N-methyl-S-phenylsulfonimidoyl]cyclohexyl)pent-4-en-1-ol; With 1H-imidazole; In N,N-dimethyl-formamide; at 0 ℃; for 1h; Inert atmosphere;

triethylsilyl chloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 20h; Inert atmosphere;
DOI:10.1002/chem.201103060