(Z)-methyl N'-cyano-N-(3,5-dichloro-4-(phenylthio)phenyl)carbamimidothioate

Base Information

Chemical Name:(Z)-methyl N'-cyano-N-(3,5-dichloro-4-(phenylthio)phenyl)carbamimidothioate
CAS No.:1620878-53-6
Molecular Formula:C₁₅H₁₁Cl₂N₃S₂
Molecular Weight:368.31
Hs Code.:

Synonyms:(Z)-methyl N'-cyano-N-(3,5-dichloro-4-(phenylthio)phenyl)carbamimidothioate

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Chemical Property of (Z)-methyl N'-cyano-N-(3,5-dichloro-4-(phenylthio)phenyl)carbamimidothioate

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Technology Process of (Z)-methyl N'-cyano-N-(3,5-dichloro-4-(phenylthio)phenyl)carbamimidothioate

There total 5 articles about (Z)-methyl N'-cyano-N-(3,5-dichloro-4-(phenylthio)phenyl)carbamimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620782-81-1
1,3-dichloro-5-isothiocyanato-2-phenylsulfanylbenzene

: 19981-17-0,20611-81-8,123092-13-7,17292-62-5
sodium cyanamide

: 74-88-4
methyl iodide

: 1620878-53-6
(Z)-methyl N'-cyano-N-(3,5-dichloro-4-(phenylthio)phenyl)carbamimidothioate

Guidance literature:: sodium cyanamide; With sodium methylate; In methanol; at 20 ℃; for 0.416667h; Inert atmosphere;

1,3-dichloro-5-isothiocyanato-2-phenylsulfanylbenzene; In methanol; toluene; at 20 ℃; for 1h; Inert atmosphere;

methyl iodide; In methanol; toluene; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

: 108-98-5
thiophenol

: 1620878-53-6
(Z)-methyl N'-cyano-N-(3,5-dichloro-4-(phenylthio)phenyl)carbamimidothioate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 100 °C

2.1: iron; ammonium chloride / water; methanol / 1.5 h / Reflux

3.1: dichloromethane / 20 °C

4.1: sodium methylate / methanol / 0.42 h / 20 °C / Inert atmosphere

4.2: 1 h / 20 °C / Inert atmosphere

4.3: 16 h / 20 °C / Inert atmosphere

With sodium methylate; iron; potassium carbonate; ammonium chloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 180253-72-9
(2,6-dichloro-4-nitrophenyl)(phenyl)sulfane

: 1620878-53-6
(Z)-methyl N'-cyano-N-(3,5-dichloro-4-(phenylthio)phenyl)carbamimidothioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: iron; ammonium chloride / water; methanol / 1.5 h / Reflux

2.1: dichloromethane / 20 °C

3.1: sodium methylate / methanol / 0.42 h / 20 °C / Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

3.3: 16 h / 20 °C / Inert atmosphere

With sodium methylate; iron; ammonium chloride; In methanol; dichloromethane; water;