C₅₄H₆₇NO₁₄Si

Base Information

Chemical Name:C₅₄H₆₇NO₁₄Si
CAS No.:204981-05-5
Molecular Formula:C₅₄H₆₇NO₁₄Si
Molecular Weight:982.21
Hs Code.:

C<sub>54</sub>H<sub>67</sub>NO<sub>14</sub>Si

Synonyms:C₅₄H₆₇NO₁₄Si

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Chemical Property of C₅₄H₆₇NO₁₄Si

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Technology Process of C₅₄H₆₇NO₁₄Si

There total 9 articles about C₅₄H₆₇NO₁₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 204981-04-4
C₅₄H₆₇NO₁₃SSi

: 204981-05-5
C₅₄H₆₇NO₁₄Si

Guidance literature:: With methanol; 4 A molecular sieve; iodine; for 7h;
DOI:10.1016/S0960-894X(01)00280-3

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 204981-05-5
C₅₄H₆₇NO₁₄Si

Guidance literature:: Multi-step reaction with 7 steps

1: imidazole / dimethylformamide / 24 h / 0 °C

2: iPr₂NEt; DMAP / CH₂Cl₂ / 24 h / -40 - 0 °C

3: TPAP; NMO; 4 Angstroem sieves / CH₂Cl₂

4: 50 percent / KHMDS / tetrahydrofuran / -40 °C

5: 83 percent / 48 percent HF; pyridine / acetonitrile / 3 h / 0 °C

6: 80 percent / Bz₂O₂ / acetonitrile / 0.5 h / 0 °C

7: 75 percent / I₂; 4 Angstroem sieves; MeOH / 7 h

With pyridine; 1H-imidazole; methanol; dmap; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; hydrogen fluoride; iodine; potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine; dibenzoyl peroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0960-894X(01)00280-3

Reference yield:

: 148121-24-8
10-deacetoxy-paclitaxel

: 204981-05-5
C₅₄H₆₇NO₁₄Si

Guidance literature:: Multi-step reaction with 7 steps

1: imidazole / dimethylformamide / 24 h / 0 °C

2: iPr₂NEt; DMAP / CH₂Cl₂ / 24 h / -40 - 0 °C

3: TPAP; NMO; 4 Angstroem sieves / CH₂Cl₂

4: 50 percent / KHMDS / tetrahydrofuran / -40 °C

5: 83 percent / 48 percent HF; pyridine / acetonitrile / 3 h / 0 °C

6: 80 percent / Bz₂O₂ / acetonitrile / 0.5 h / 0 °C

7: 75 percent / I₂; 4 Angstroem sieves; MeOH / 7 h

With pyridine; 1H-imidazole; methanol; dmap; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; hydrogen fluoride; iodine; potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine; dibenzoyl peroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0960-894X(01)00280-3