Cyclopropane-1,1,2,2,3,3-hexacarboxylicacidhexamethylester

Base Information

• Chemical Name: Cyclopropane-1,1,2,2,3,3-hexacarboxylicacidhexamethylester
• CAS No.: 109777-05-1
• Molecular Formula: C15H18 O12
• Molecular Weight: 390.301
• Hs Code.: 2917209090
• Mol file: 109777-05-1.mol

Synonyms:Cyclopropanehexacarboxylicacid, hexamethyl ester (9CI); Hexacarbomethoxycyclopropane; Hexamethylcyclopropanehexacarboxylate

Chemical Property of Cyclopropane-1,1,2,2,3,3-hexacarboxylicacidhexamethylester

Chemical Property:

• Vapor Pressure: 1.07E-07mmHg at 25°C
• Melting Point: 235-237 °C
• Refractive Index: 1.489
• Boiling Point: 432.9°Cat760mmHg
• Flash Point: 188.3°C
• PSA: 157.80000
• Density: 1.423g/cm³
• LogP: -2.00280

Purity/Quality:

97% ^*data from raw suppliers

Cyclopropane-1,1,2,2,3,3-hexacarboxylicAcidHexamethylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclopropane-1,1,2,2,3,3-hexacarboxylicacidhexamethylester

There total 5 articles about Cyclopropane-1,1,2,2,3,3-hexacarboxylicacidhexamethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

propane-1,1,2,2,3,3-hexacarboxylic acid hexamethyl ester (28781-91-1) → hexanethyl ester of cyclopropanehexacarboxylic acid (109777-05-1)

Guidance literature:

With sodium iodide; In methanol; at 45 ℃; electrolysis, 220 mA/cm², 7.3 F/mole, Pt anode, iron cathode;

DOI:10.1007/BF00953888

Reference yield: 60.0%

malonic acid dimethyl ester (108-59-8) → tetramethyl ethane-1,1,2,2-tetracarboxylate (5464-22-2) + Dimethoxymalonic acid dimethyl ester (29340-86-1) + hexanethyl ester of cyclopropanehexacarboxylic acid (109777-05-1)

Guidance literature:

With potassium bromide; at 50 ℃; electrolysis, a platinum anode, iron cathode, 220 mA/cm² current density;

DOI:10.1007/BF00954639

Reference yield: 24.0%

propane-1,1,2,2,3,3-hexacarboxylic acid hexamethyl ester (28781-91-1) → hexanethyl ester of cyclopropanehexacarboxylic acid (109777-05-1) + Hexamethyl ester of 1-bromopropane-1,1,2,2,3,3-hexacarboxylic acid (133455-79-5)

Guidance literature:

With sodium bromide; In methanol; at 20 ℃; electrolysis (Pt vs. Fe) with current density of 220 mA/cm², amount 2F;

DOI:10.1007/BF01184531

upstream raw materials:

propane-1,1,2,2,3,3-hexacarboxylic acid hexamethyl ester

malonic acid dimethyl ester

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