1-(2-Amino-6-methylphenyl)-2-chloroethanone

Base Information

Chemical Name:1-(2-Amino-6-methylphenyl)-2-chloroethanone
CAS No.:109532-24-3
Molecular Formula:C9H10 Cl N O
Molecular Weight:183.637
Hs Code.:
DSSTox Substance ID:DTXSID70551670
Wikidata:Q82431459
Mol file:109532-24-3.mol

Synonyms:109532-24-3;1-(2-Amino-6-methylphenyl)-2-chloroethanone;Ethanone, 1-(2-amino-6-methylphenyl)-2-chloro- (9CI);DTXSID70551670;1-(2-Amino-6-methylphenyl)-2-chloroethan-1-one

Suppliers and Price of 1-(2-Amino-6-methylphenyl)-2-chloroethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-(2-Amino-6-methylphenyl)-2-chloroethanone

Chemical Property:

PSA：43.09000
LogP:2.57990
XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:183.0450916
Heavy Atom Count:12
Complexity:172

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=CC=C1)N)C(=O)CCl

Technology Process of 1-(2-Amino-6-methylphenyl)-2-chloroethanone

There total 3 articles about 1-(2-Amino-6-methylphenyl)-2-chloroethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109532-31-2
2-(Acetylamino)-α-chlor-6-methylacetophenon

: 109532-24-3
2-Amino-α-chlor-6-methylacetophenon

Guidance literature:: With hydrogenchloride; In methanol; for 0.5h; Heating;

Reference yield:

: 108-44-1
1-amino-3-methylbenzene

: 109532-24-3
2-Amino-α-chlor-6-methylacetophenon

Guidance literature:: Multi-step reaction with 2 steps

1: 1) BCl₃, ZnCl₂ / 1) CH₂Cl₂, 48 h, reflux; 2) CCl₄, 80 degC

2: HCl / methanol / 0.5 h / Heating

With hydrogenchloride; boron trichloride; zinc(II) chloride; In methanol;

Reference yield:

: 107-14-2
chloroacetonitrile

: 108-44-1
1-amino-3-methylbenzene

: 109532-23-2
2-Amino-α-chlor-4-methylacetophenon

: 109532-24-3
2-Amino-α-chlor-6-methylacetophenon

Guidance literature:: With boron trichloride; zinc(II) chloride; In dichloromethane; for 48h; Yield given. Yields of byproduct given; Heating;