phenyl ((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)carbamate

Base Information

• Chemical Name: phenyl ((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)carbamate
• CAS No.: 1620293-50-6
• Molecular Formula: C₂₂H₂₂N₄O₄
• Molecular Weight: 406.441

Synonyms:phenyl ((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)carbamate

Chemical Property of phenyl ((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)carbamate

Chemical Property:

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Technology Process of phenyl ((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)carbamate

There total 1 articles about phenyl ((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methanamine hydrochloride (1620293-11-9) + phenyl chloroformate (1885-14-9) → phenyl ((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)carbamate (1620293-50-6)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

Reference yield: 17.1%

phenyl ((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)carbamate (1620293-50-6) + 6,7-dihydro-4H-thieno[3,2-c]pyridine hydrochloride (28783-41-7) → N-((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)-6,7-dihydrothieno[3,2-c]pyridine-5(4H)-carboxamide (1620291-21-5)

Guidance literature:

With triethylamine; In dimethyl sulfoxide; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

phenyl ((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)carbamate (1620293-50-6) + 1,2,3,4-tetrahydropyrrolo[1,2-a]pyrazine trifluoroacetate (1620295-14-8) → N-((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)-3,4-dihydropyrrolo[1,2-a]pyrazine-2(1H)-carboxamide (1620291-20-4)

Guidance literature:

With triethylamine; In dimethyl sulfoxide; at 20 ℃; for 12h;

upstream raw materials:

(5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methanamine hydrochloride

phenyl chloroformate

Downstream raw materials:

N-((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)-3,4-dihydropyrrolo[1,2-a]pyrazine-2(1H)-carboxamide

N-((5-((2-(1-methyl-1H-pyrazol-4-yl)phenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)-6,7-dihydrothieno[3,2-c]pyridine-5(4H)-carboxamide

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