4-benzyloxy-3-nitrobenzoic acid isopropyl ester

Base Information

Chemical Name:4-benzyloxy-3-nitrobenzoic acid isopropyl ester
CAS No.:1373491-26-9
Molecular Formula:C₁₇H₁₇NO₅
Molecular Weight:315.326
Hs Code.:

Synonyms:4-benzyloxy-3-nitrobenzoic acid isopropyl ester

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Chemical Property of 4-benzyloxy-3-nitrobenzoic acid isopropyl ester

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Technology Process of 4-benzyloxy-3-nitrobenzoic acid isopropyl ester

There total 1 articles about 4-benzyloxy-3-nitrobenzoic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.5%

: 17903-89-8
3-nitro-4-phenylmethoxybenzoic acid

: 75-26-3
isopropyl bromide

: 1373491-26-9
4-benzyloxy-3-nitrobenzoic acid isopropyl ester

Guidance literature:: With tetradecyl(trihexyl)phosphonium bistriflamide; N-ethyl-N,N-diisopropylamine; at 40 ℃; for 12h;

Reference yield: 92.4%

: 1373491-26-9
4-benzyloxy-3-nitrobenzoic acid isopropyl ester

: 1216156-34-1
isopropyl 3-amino-4-hydroxybenzoate

Guidance literature:: With hydrogen; 5%-palladium/activated carbon; In methanol; at 20 ℃;

Reference yield:

: 1373491-26-9
4-benzyloxy-3-nitrobenzoic acid isopropyl ester

: 1373491-25-8
3-[2-(4-adamantan-1-ylphenoxy)acetylamino]-4-hydroxybenzoic acid isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / 5%-palladium/activated carbon / methanol / 20 °C

2: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 5%-palladium/activated carbon; In methanol; N,N-dimethyl-formamide;