1-(3,4-dimethoxyphenyl)-c-4--N-methylamino>-r-cyclohexanecarbonitrile

Base Information

Chemical Name:1-(3,4-dimethoxyphenyl)-c-4--N-methylamino>-r-cyclohexanecarbonitrile
CAS No.:133648-48-3
Molecular Formula:C₂₆H₃₄N₂O₄
Molecular Weight:438.567
Hs Code.:

1-(3,4-dimethoxyphenyl)-c-4-<N-<2-(3,4-dimethoxyphenyl)ethyl>-N-methylamino>-r-cyclohexanecarbonitrile

Synonyms:1-(3,4-dimethoxyphenyl)-c-4--N-methylamino>-r-cyclohexanecarbonitrile

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Chemical Property of 1-(3,4-dimethoxyphenyl)-c-4--N-methylamino>-r-cyclohexanecarbonitrile

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Technology Process of 1-(3,4-dimethoxyphenyl)-c-4--N-methylamino>-r-cyclohexanecarbonitrile

There total 11 articles about 1-(3,4-dimethoxyphenyl)-c-4--N-methylamino>-r-cyclohexanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 40173-90-8
3,4-dimethoxyphenethyl bromide

: 133648-68-7
1-(3,4-dimethoxyphenyl)-c-4-(methylamino)-r-1-cyclohexanecarbonitrile

: 133648-48-3
1-(3,4-dimethoxyphenyl)-c-4--N-methylamino>-r-cyclohexanecarbonitrile

Guidance literature:: With potassium carbonate; In acetonitrile; for 44h; Heating;
DOI:10.1021/jm00111a043

Reference yield: 52.0%

: 3490-06-0
N-methylhomoveratrylamine

: 133648-57-4
1-(3,4-dimethoxyphenyl)-t-4-bromo-r-1-cyclohexanecarbonitrile

: 133648-60-9
4-(3,4-dimethoxyphenyl)-4-cyano-1-cyclohexene

: 133648-48-3
1-(3,4-dimethoxyphenyl)-c-4--N-methylamino>-r-cyclohexanecarbonitrile

Guidance literature:: In xylene; for 6h; Heating;
DOI:10.1021/jm00111a043

Reference yield:

: 69299-13-4
1-(3,4-dimethoxyphenyl)-4-hydroxy-1-cyclohexanecarbonitrile

: 133648-48-3
1-(3,4-dimethoxyphenyl)-c-4--N-methylamino>-r-cyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: PBr₃ / 1.) RT, 24 h, 2.) 80 deg C, 4 h

2: 52 percent / xylene / 6 h / Heating

With phosphorus tribromide; In xylene;
DOI:10.1021/jm00111a043