2-(Aminomethyl)-3-chloroaniline

Base Information

Chemical Name:2-(Aminomethyl)-3-chloroaniline
CAS No.:109319-83-7
Molecular Formula:C7H9 Cl N2
Molecular Weight:156.615
Hs Code.:2921590090
DSSTox Substance ID:DTXSID30547115
Wikidata:Q82425141
Mol file:109319-83-7.mol

Synonyms:2-(Aminomethyl)-3-chloroaniline;109319-83-7;Benzenemethanamine, 2-amino-6-chloro-;SCHEMBL2833792;DTXSID30547115;AKOS011790559;CS-0284164;F87687;EN300-1255885

Suppliers and Price of 2-(Aminomethyl)-3-chloroaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Biosynth Carbosynth
2-Amino-6-chlorobenzylamine - 94%
1 g
$ 300.00

Biosynth Carbosynth
2-Amino-6-chlorobenzylamine - 94%
500 mg
$ 180.00

Biosynth Carbosynth
2-Amino-6-chlorobenzylamine - 94%
250 mg
$ 100.00

Biosynth Carbosynth
2-Amino-6-chlorobenzylamine - 94%
2 g
$ 500.00

American Custom Chemicals Corporation
2-AMINO-6-CHLOROBENZYLAMINE 95.00%
5MG
$ 503.27

Alichem
2-Amino-6-chlorobenzylamine
1g
$ 1519.80

Alichem
2-Amino-6-chlorobenzylamine
500mg
$ 790.55

Alichem
2-Amino-6-chlorobenzylamine
250mg
$ 494.40

Total 2 raw suppliers

Chemical Property of 2-(Aminomethyl)-3-chloroaniline

Chemical Property:

PSA：52.04000
LogP:2.66240
XLogP3:1.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:156.0454260
Heavy Atom Count:10
Complexity:108

Purity/Quality:

99% ^*data from raw suppliers

2-Amino-6-chlorobenzylamine - 94% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)Cl)CN)N

Technology Process of 2-(Aminomethyl)-3-chloroaniline

There total 5 articles about 2-(Aminomethyl)-3-chloroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.4%

: 6575-11-7
2-amino-6-chlorobenzonitrile

: 109319-83-7
2-amino-6-chlorobenzylamine

Guidance literature:: 2-amino-6-chlorobenzonitrile; With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 - 30 ℃; for 1h; Heating / reflux;

With water; In tetrahydrofuran; at 0 - 10 ℃;

Reference yield:

: 101252-73-7
2-Chlor-6-nitrobenzylamin

: 109319-83-7
2-amino-6-chlorobenzylamine

Guidance literature:: With nickel; In ethanol; Yield given; Ambient temperature;
DOI:10.1002/hlca.19860690816

Reference yield:

: 83-42-1
6-chloro-2-nitrotoluene

: 109319-83-7
2-amino-6-chlorobenzylamine

Guidance literature:: Multi-step reaction with 4 steps

1: N-bromosuccinimide

2: dimethylformamide / 2 h / Ambient temperature

3: 1.) hydrazin-hydrate, 2.) HCl / 1.) MeOH, 1 h, reflux, 2.) H₂O, MeOH

4: Raney-Ni / ethanol / Ambient temperature

With hydrogenchloride; N-Bromosuccinimide; nickel; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19860690816