[(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Ni(H₂O)(benzoato)2]

Base Information

• Chemical Name: [(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Ni(H₂O)(benzoato)2]
• CAS No.: 872993-25-4
• Molecular Formula: C₄₄H₃₈N₄NiO₅
• Molecular Weight: 761.5

Synonyms:[(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Ni(H₂O)(benzoato)2]

Chemical Property of [(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Ni(H₂O)(benzoato)2]

Chemical Property:

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Technology Process of [(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Ni(H₂O)(benzoato)2]

There total 4 articles about [(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Ni(H₂O)(benzoato)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)-methyl)amine (167897-42-9) + ([Ni(PhC(O)C(O)C(O)Ph(H2O)]*H2O*0.25CH3CN)6 → [(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Ni(H2O)(benzoato)2] (872993-25-4)

Guidance literature:

With O₂; In acetonitrile; byproducts: CO; soln. of Ni complex and amine in MeCN exposed to O2;

DOI:10.1021/ic100775m

Reference yield:

[(6-Ph2TPA)Ni(PhC(O)C(OH)C(O)Ph)]ClO4 → [(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Ni(H2O)(benzoato)2] (872993-25-4)

Guidance literature:

With (CH₃)4NOH*6H₂O; O₂; In acetonitrile; byproducts: CO; Ni complex treated with ammonium salt under anaerobic conditions; soln. exposed to O2;

DOI:10.1021/ic100775m

Reference yield:

[(6-Ph2TPA)Ni(PhC(O)C(OH)C(O)Ph)]ClO4 + oxygen (80937-33-3) → [(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Ni(H2O)(benzoato)2] (872993-25-4)

Guidance literature:

With Me₄NOH*5H₂O; In acetonitrile; byproducts: CO, PhC(O)C(O)Ph; Ni complex reacted with O2 in MeCN in presence of Me4NOH (1 equiv.);

DOI:10.1021/ic061316w

upstream raw materials:

sodium benzoate

N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)-methyl)amine

oxygen

Downstream raw materials:

[(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Ni(H₂O)(benzoato)]ClO₄

[(6-Ph₂TPA)Ni(O₂CPh)]ClO₄

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