2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethyl 4-nitrophenyl carbonate

Base Information

• Chemical Name: 2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethyl 4-nitrophenyl carbonate
• CAS No.: 1256781-54-0
• Molecular Formula: C₃₀H₂₇N₇O₉
• Molecular Weight: 629.586
• Mol file: 1256781-54-0.mol

Synonyms:2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethyl 4-nitrophenyl carbonate

Chemical Property of 2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethyl 4-nitrophenyl carbonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethyl 4-nitrophenyl carbonate

There total 1 articles about 2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethyl 4-nitrophenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethanol (1256781-53-9) + 4-Nitrophenyl chloroformate (7693-46-1) → 2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethyl 4-nitrophenyl carbonate (1256781-54-0)

Guidance literature:

With pyridine; In dichloromethane; for 2h; Inert atmosphere;

DOI:10.1039/c0ob00322k

Reference yield: 42.0%

2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethyl 4-nitrophenyl carbonate (1256781-54-0) + C75H108N13O21Pol → C84H121N19O25

Guidance literature:

C₇₅H₁₀₈N₁₃O₂₁Pol; With piperidine; at 20 ℃; for 1h; Inert atmosphere; solid phase reaction;

2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethyl 4-nitrophenyl carbonate; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; Inert atmosphere; solid phase reaction;

With chlorotriisopropylsilane; water; trifluoroacetic acid; for 2h; solid phase reaction;

DOI:10.1039/c0ob00322k

upstream raw materials:

2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethanol

4-Nitrophenyl chloroformate