2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethanol

Base Information

• Chemical Name: 2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethanol
• CAS No.: 1256781-53-9
• Molecular Formula: C₂₃H₂₄N₆O₅
• Molecular Weight: 464.481
• Mol file: 1256781-53-9.mol

Synonyms:2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethanol

Chemical Property of 2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethanol

There total 1 articles about 2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

N-(2-hydroxyethyl)-N-methylaminobenzene (93-90-3) + (E)-2,5-dimethoxy-4-((4-nitrophenyl)diazenyl)aniline (6358-51-6) → 2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethanol (1256781-53-9)

Guidance literature:

(E)-2,5-dimethoxy-4-((4-nitrophenyl)diazenyl)aniline; With nitrosyl sulfonic acid; sulfuric acid; In water; at 20 ℃; Cooling with ice;

With tetrafluoroboric acid; Cooling with ice;

N-(2-hydroxyethyl)-N-methylaminobenzene; In tetrahydrofuran;

DOI:10.1039/c0ob00322k

Reference yield: 97.0%

2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethanol (1256781-53-9) + 4-Nitrophenyl chloroformate (7693-46-1) → 2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethyl 4-nitrophenyl carbonate (1256781-54-0)

Guidance literature:

With pyridine; In dichloromethane; for 2h; Inert atmosphere;

DOI:10.1039/c0ob00322k

upstream raw materials:

N-(2-hydroxyethyl)-N-methylaminobenzene

(E)-2,5-dimethoxy-4-((4-nitrophenyl)diazenyl)aniline

Downstream raw materials:

2-((4-((E)-(2,5-dimethoxy-4-((E)-(4-nitrophenyl)diazenyl)phenyl)diazenyl)phenyl)(methyl)amino)ethyl 4-nitrophenyl carbonate