(3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.1(3,6).1(5,19).0(9,11).0(31,35)]octatriaconta-1⁽³⁴⁾,12,26,28,30,32,35-heptaene-9-carboxamide

Base Information

• Chemical Name: (3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.1(3,6).1(5,19).0(9,11).0(31,35)]octatriaconta-1⁽³⁴⁾,12,26,28,30,32,35-heptaene-9-carboxamide
• CAS No.: 1025366-82-8
• Molecular Formula: C₄₅H₅₃N₅O₉S
• Molecular Weight: 840.01

Synonyms:(3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.1(3,6).1(5,19).0(9,11).0(31,35)]octatriaconta-1⁽³⁴⁾,12,26,28,30,32,35-heptaene-9-carboxamide

Chemical Property of (3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.1(3,6).1(5,19).0(9,11).0(31,35)]octatriaconta-1⁽³⁴⁾,12,26,28,30,32,35-heptaene-9-carboxamide

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Technology Process of (3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.1(3,6).1(5,19).0(9,11).0(31,35)]octatriaconta-1⁽³⁴⁾,12,26,28,30,32,35-heptaene-9-carboxamide

There total 2 articles about (3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.1(3,6).1(5,19).0(9,11).0(31,35)]octatriaconta-1⁽³⁴⁾,12,26,28,30,32,35-heptaene-9-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

cyclopropanesulphonamide (154350-29-5) + (3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.1(3,6).1(5,19).0(9,11).0(31,35)]octatriaconta-1(34),12,26,28,30,32,35-heptaene-9-carboxylic acid → (3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.1(3,6).1(5,19).0(9,11).0(31,35)]octatriaconta-1(34),12,26,28,30,32,35-heptaene-9-carboxamide (1025366-82-8)

Guidance literature:

(3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.1(3,6).1(5,19).0(9,11).0(31,35)]octatriaconta-1⁽³⁴⁾,12,26,28,30,32,35-heptaene-9-carboxylic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 40 ℃; for 5h;

cyclopropanesulphonamide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 40 ℃; for 18h;

DOI:10.1002/anie.200803298

Reference yield:

cyclopropanesulphonamide (154350-29-5) + (3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1(35),12,26,28,30,31,33,35-octaene-9-carboxylic acid (1025366-80-6) → (3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.1(3,6).1(5,19).0(9,11).0(31,35)]octatriaconta-1(34),12,26,28,30,32,35-heptaene-9-carboxamide (1025366-82-8)

Guidance literature:

(3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxylic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 40 ℃; for 5h;

cyclopropanesulphonamide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 40 ℃; for 18h;

upstream raw materials:

cyclopropanesulphonamide

(3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxylic acid

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