1-allyl-4-{5-[4-(dihexylamino)phenyl] thiophene-2-yl} pyridinium iodide

Base Information

Chemical Name:1-allyl-4-{5-[4-(dihexylamino)phenyl] thiophene-2-yl} pyridinium iodide
CAS No.:1236567-81-9
Molecular Formula:C₃₀H₄₁N₂S*I
Molecular Weight:588.639
Hs Code.:

Synonyms:1-allyl-4-{5-[4-(dihexylamino)phenyl] thiophene-2-yl} pyridinium iodide

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Chemical Property of 1-allyl-4-{5-[4-(dihexylamino)phenyl] thiophene-2-yl} pyridinium iodide

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Technology Process of 1-allyl-4-{5-[4-(dihexylamino)phenyl] thiophene-2-yl} pyridinium iodide

There total 4 articles about 1-allyl-4-{5-[4-(dihexylamino)phenyl] thiophene-2-yl} pyridinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 556-56-9
allyl iodid

: 1236567-70-6
N,N-dihexyl-4-(5-(pyridin-4-yl)thiophene-2-yl)benzenamine

: 1236567-81-9
1-allyl-4-{5-[4-(dihexylamino)phenyl] thiophene-2-yl} pyridinium iodide

Guidance literature:: In dichloromethane; at 35 ℃; for 0.5h;

Reference yield:

: 638-45-9
1-Iodohexane

: 1236567-81-9
1-allyl-4-{5-[4-(dihexylamino)phenyl] thiophene-2-yl} pyridinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 22 h / 90 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; methanol / 0.5 h / 70 °C / Inert atmosphere

2.2: 9 h / 70 °C / Inert atmosphere

3.1: dichloromethane / 0.5 h / 35 °C

With sodium carbonate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 540-37-4
p-aminoiodobenzene

: 1236567-81-9
1-allyl-4-{5-[4-(dihexylamino)phenyl] thiophene-2-yl} pyridinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 22 h / 90 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; methanol / 0.5 h / 70 °C / Inert atmosphere

2.2: 9 h / 70 °C / Inert atmosphere

3.1: dichloromethane / 0.5 h / 35 °C

With sodium carbonate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;