C₃₈H₅₀N₆O₉

Base Information

Chemical Name:C₃₈H₅₀N₆O₉
CAS No.:1425940-89-1
Molecular Formula:C₃₈H₅₀N₆O₉
Molecular Weight:734.85
Hs Code.:

C<sub>38</sub>H<sub>50</sub>N<sub>6</sub>O<sub>9</sub>

Synonyms:C₃₈H₅₀N₆O₉

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Chemical Property of C₃₈H₅₀N₆O₉

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Technology Process of C₃₈H₅₀N₆O₉

There total 7 articles about C₃₈H₅₀N₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1425940-84-6
(S)-methyl-2-methyl-2-(2-(pyrrolidine-2-carboxamido)benzamido)propanoate

: 1425940-87-9
C₂₁H₂₇N₃O₅

: 1425940-89-1
C₃₈H₅₀N₆O₉

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1h; Molecular sieve;
DOI:10.1021/ol4002762

Reference yield:

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 1425940-89-1
C₃₈H₅₀N₆O₉

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C

2.1: triethylamine / dichloromethane / 5 h / 20 °C / Cooling with ice

3.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 5 h / 3102.97 Torr

4.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 0.42 h / 0 °C / Inert atmosphere

4.2: 8 h / Inert atmosphere; Reflux

5.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Molecular sieve

With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ol4002762

Reference yield:

: 610-14-0
2-nitrobenzyl chloride

: 1425940-89-1
C₃₈H₅₀N₆O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 5 h / 20 °C / Cooling with ice

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 5 h / 3102.97 Torr

3.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 0.42 h / 0 °C / Inert atmosphere

3.2: 8 h / Inert atmosphere; Reflux

4.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Molecular sieve

With palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ol4002762