2,2'-[{[4-(chloromethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

Base Information

Chemical Name:2,2'-[{[4-(chloromethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)
CAS No.:1259039-33-2
Molecular Formula:C₂₀H₂₈ClN₇O₄S₂
Molecular Weight:530.072
Hs Code.:

Synonyms:2,2'-[{[4-(chloromethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

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Chemical Property of 2,2'-[{[4-(chloromethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

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Technology Process of 2,2'-[{[4-(chloromethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

There total 3 articles about 2,2'-[{[4-(chloromethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1259039-32-1
2,2'-[{[4-(hydroxymethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

: 1259039-33-2
2,2'-[{[4-(chloromethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

Guidance literature:: With methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

Reference yield:

: 937074-59-4
2,2'-[{[4-(diethoxymethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

: 1259039-33-2
2,2'-[{[4-(chloromethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; water / ethyl acetate / 0.05 h / 20 °C

2: sodium tetrahydroborate; methanol / tetrahydrofuran / 2 h / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine; methanesulfonyl chloride; lithium chloride / tetrahydrofuran / 1 h / 0 - 20 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; water; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; ethyl acetate;

Reference yield:

: 1259039-31-0
2,2'-[[(4-formylbenzyl)imino]bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

: 1259039-33-2
2,2'-[{[4-(chloromethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; methanol / tetrahydrofuran / 2 h / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine; methanesulfonyl chloride; lithium chloride / tetrahydrofuran / 1 h / 0 - 20 °C

With methanol; sodium tetrahydroborate; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran;