N¹-diphenyloxyphosphonate-N¹-methylhydrazide

Base Information

Chemical Name:N¹-diphenyloxyphosphonate-N¹-methylhydrazide
CAS No.:54529-79-2
Molecular Formula:C₁₃H₁₅N₂O₃P
Molecular Weight:278.247
Hs Code.:

N<sup>1</sup>-diphenyloxyphosphonate-N<sup>1</sup>-methylhydrazide

Synonyms:N¹-diphenyloxyphosphonate-N¹-methylhydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹-diphenyloxyphosphonate-N¹-methylhydrazide

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Technology Process of N¹-diphenyloxyphosphonate-N¹-methylhydrazide

There total 1 articles about N¹-diphenyloxyphosphonate-N¹-methylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60-34-4
methylhydrazine

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 54529-79-2
N¹-diphenyloxyphosphonate-N¹-methylhydrazide

Guidance literature:: With sodium carbonate;
DOI:10.1002/jps.2600631114

Reference yield: 89.0%

: 54529-79-2
N¹-diphenyloxyphosphonate-N¹-methylhydrazide

: 120384-18-1
4-azido-2,3,5,6-tetrafluorobenzaldehyde

: N'-[1-(4-Azido-2,3,5,6-tetrafluoro-phenyl)-meth-(Z)-ylidene]-N-methyl-phosphorohydrazidic acid diphenyl ester

Guidance literature:: In ethanol; at 0 ℃; for 0.5h;
DOI:10.1021/jo981458a

Reference yield: 85.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 54529-79-2
N¹-diphenyloxyphosphonate-N¹-methylhydrazide

: 154719-37-6
(1-methylphosphorohydrazidic acid O,O-diphenylester)palladium dichloride

Guidance literature:: In dichloromethane; N2-atmosphere; addn. of stoich. amt. of Pd-complex to ligand (25°C, stirring; pptn.), stirring (2 h); filtration, washing (hexane, Et2O), recrystn. (boiling MeCN); elem. anal.;