dimethyl phospnonate

Base Information

• Chemical Name: dimethyl phospnonate
• CAS No.: 127787-64-8
• Molecular Formula: C₂₃H₂₅O₅P
• Molecular Weight: 412.422

Synonyms:dimethyl phospnonate

Chemical Property of dimethyl phospnonate

Chemical Property:

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Technology Process of dimethyl phospnonate

There total 1 articles about dimethyl phospnonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4,4'-dimethoxytrityl chloride (40615-36-9) + phosphorous acid trimethyl ester (121-45-9) → dimethyl phospnonate (127787-64-8)

Guidance literature:

In benzene; for 2h; Reflux;

DOI:10.1021/ja8020999

Reference yield: 73.0%

dimethyl phospnonate (127787-64-8) → phosphonic acid (94967-76-7)

Guidance literature:

With chloro-trimethyl-silane; lithium bromide; In acetonitrile; at 60 ℃; for 5h;

DOI:10.1246/bcsj.63.453

upstream raw materials:

4,4'-dimethoxytrityl chloride

phosphorous acid trimethyl ester

Downstream raw materials:

phosphonic acid

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