<α-(N-benzyloxycarbonyl N-methyl amino) methoxy-4 benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

Base Information

Chemical Name:<α-(N-benzyloxycarbonyl N-methyl amino) methoxy-4 benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle
CAS No.:122082-71-7
Molecular Formula:C₂₇H₃₅NO₅
Molecular Weight:453.579
Hs Code.:

Synonyms:<α-(N-benzyloxycarbonyl N-methyl amino) methoxy-4 benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

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Chemical Property of <α-(N-benzyloxycarbonyl N-methyl amino) methoxy-4 benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

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Technology Process of <α-(N-benzyloxycarbonyl N-methyl amino) methoxy-4 benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

There total 5 articles about <α-(N-benzyloxycarbonyl N-methyl amino) methoxy-4 benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 122082-70-6
<α-(N-benzyloxycarbonyl amino) p-methoxy benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

: 74-88-4
methyl iodide

: 122082-71-7
<α-(N-benzyloxycarbonyl N-methyl amino) methoxy-4 benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 3h;
DOI:10.1016/0223-5234(88)90091-8

Reference yield:

: 57078-08-7,57129-25-6,61490-75-3,93781-25-0,116696-95-8,116696-96-9,145415-55-0,145415-56-1,82801-37-4
acide cis-p-anisoyl-3 trimethyl-1,2,2 cyclopentane carboxylique

: 122082-71-7
<α-(N-benzyloxycarbonyl N-methyl amino) methoxy-4 benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

Guidance literature:: Multi-step reaction with 5 steps

1: diethyl ether

2: 77 percent / NH₂OH*HCl, pyridine / ethanol / 4 h / Heating

3: 47 percent / Al/Hg, 5percent HgCl / ethanol; H₂O / 2 h

4: 97 percent / Na / H₂O / 40 h / 0 - 20 °C

5: 77 percent / NaH / dimethylformamide / 3 h

With pyridine; aluminum amalgam; hydroxylamine hydrochloride; sodium; sodium hydride; mercury(II) chloride; In diethyl ether; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(88)90091-8

Reference yield:

: 93740-32-0,93740-33-1,122082-22-8
ester methylique de l'acide cis-p-anisoyl-3 trimethyl-1,2,2 cyclopentane carboxylique

: 122082-71-7
<α-(N-benzyloxycarbonyl N-methyl amino) methoxy-4 benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / NH₂OH*HCl, pyridine / ethanol / 4 h / Heating

2: 47 percent / Al/Hg, 5percent HgCl / ethanol; H₂O / 2 h

3: 97 percent / Na / H₂O / 40 h / 0 - 20 °C

4: 77 percent / NaH / dimethylformamide / 3 h

With pyridine; aluminum amalgam; hydroxylamine hydrochloride; sodium; sodium hydride; mercury(II) chloride; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(88)90091-8