1-benzyl-2-[phenyl(tert-butyldimethylsilyloxy)methyl]-4,5-dihydroimidazole

Base Information

Chemical Name:1-benzyl-2-[phenyl(tert-butyldimethylsilyloxy)methyl]-4,5-dihydroimidazole
CAS No.:128993-44-2
Molecular Formula:C₂₃H₃₂N₂OSi
Molecular Weight:380.605
Hs Code.:

Synonyms:1-benzyl-2-[phenyl(tert-butyldimethylsilyloxy)methyl]-4,5-dihydroimidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyl-2-[phenyl(tert-butyldimethylsilyloxy)methyl]-4,5-dihydroimidazole

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Technology Process of 1-benzyl-2-[phenyl(tert-butyldimethylsilyloxy)methyl]-4,5-dihydroimidazole

There total 5 articles about 1-benzyl-2-[phenyl(tert-butyldimethylsilyloxy)methyl]-4,5-dihydroimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 128993-24-8
1-benzyl-2-(phenylhydroxymethyl)-4,5-dihydroimidazole

: 18162-48-6
tert-butyldimethylsilyl chloride

: 128993-44-2
1-benzyl-2-[phenyl(tert-butyldimethylsilyloxy)methyl]-4,5-dihydroimidazole

Guidance literature:: With dmap; In dichloromethane; at 20 ℃;
DOI:10.1039/c3ob40884a

Reference yield:

: 61764-86-1
1-benzyl-4,5-dihydroimidazole

: 128993-44-2
1-benzyl-2-[phenyl(tert-butyldimethylsilyloxy)methyl]-4,5-dihydroimidazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: dmap / dichloromethane / 20 °C

With dmap; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c3ob40884a

Reference yield:

: 100-52-7
benzaldehyde

: 128993-44-2
1-benzyl-2-[phenyl(tert-butyldimethylsilyloxy)methyl]-4,5-dihydroimidazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: dmap / dichloromethane / 20 °C

With dmap; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c3ob40884a