(+/-)-2-(tert-butyldimethylsilyloxy)-2-(3-(tert-butyldimethylsilyloxy)phenyl)ethanamine

Base Information

• Chemical Name: (+/-)-2-(tert-butyldimethylsilyloxy)-2-(3-(tert-butyldimethylsilyloxy)phenyl)ethanamine
• CAS No.: 1104070-56-5
• Molecular Formula: C₂₀H₃₉NO₂Si₂
• Molecular Weight: 381.706

Synonyms:(+/-)-2-(tert-butyldimethylsilyloxy)-2-(3-(tert-butyldimethylsilyloxy)phenyl)ethanamine

Chemical Property of (+/-)-2-(tert-butyldimethylsilyloxy)-2-(3-(tert-butyldimethylsilyloxy)phenyl)ethanamine

Chemical Property:

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Technology Process of (+/-)-2-(tert-butyldimethylsilyloxy)-2-(3-(tert-butyldimethylsilyloxy)phenyl)ethanamine

There total 1 articles about (+/-)-2-(tert-butyldimethylsilyloxy)-2-(3-(tert-butyldimethylsilyloxy)phenyl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

norfenefrine (536-21-0) + tert-butyldimethylsilyl chloride (18162-48-6) → (+/-)-2-(tert-butyldimethylsilyloxy)-2-(3-(tert-butyldimethylsilyloxy)phenyl)ethanamine (1104070-56-5)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 0 - 20 ℃; for 16h;

Reference yield:

6-(5-(methyltsulfinyl)-1,3,4-thiadiazol-2-yl)isoquinoline (1104070-48-5) + 6-(5-(methyltsulfonyl)-1,3,4-thiadiazol-2-yl)isoquinoline (1104070-51-0) + (+/-)-2-(tert-butyldimethylsilyloxy)-2-(3-(tert-butyldimethylsilyloxy)phenyl)ethanamine (1104070-56-5) → (+/-)-N-(2-(tert-butyldimethylsilyloxy)-2-(3-(tert-butyldimethylsilyloxy)phenyl)ethyl)-5-(isoquinolin-6-yl)-1,3,4-thiadiazol-2-amine (1104070-59-8)

Guidance literature:

In DMA; at 80 - 100 ℃; for 3h;

upstream raw materials:

norfenefrine

tert-butyldimethylsilyl chloride

Downstream raw materials:

(+/-)-N-(2-(tert-butyldimethylsilyloxy)-2-(3-(tert-butyldimethylsilyloxy)phenyl)ethyl)-5-(isoquinolin-6-yl)-1,3,4-thiadiazol-2-amine

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