2-benzyloxy-5,6,12,12a-tetrahydro-3-methoxy-9,10-methylenedioxybenz[b,g]indolizine

Base Information

Chemical Name:2-benzyloxy-5,6,12,12a-tetrahydro-3-methoxy-9,10-methylenedioxybenz[b,g]indolizine
CAS No.:7687-01-6
Molecular Formula:C₂₅H₂₃NO₄
Molecular Weight:401.462
Hs Code.:

Synonyms:2-benzyloxy-5,6,12,12a-tetrahydro-3-methoxy-9,10-methylenedioxybenz[b,g]indolizine

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Chemical Property of 2-benzyloxy-5,6,12,12a-tetrahydro-3-methoxy-9,10-methylenedioxybenz[b,g]indolizine

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Technology Process of 2-benzyloxy-5,6,12,12a-tetrahydro-3-methoxy-9,10-methylenedioxybenz[b,g]indolizine

There total 5 articles about 2-benzyloxy-5,6,12,12a-tetrahydro-3-methoxy-9,10-methylenedioxybenz[b,g]indolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 7-benzyloxy-1-(2-chloro-4,5-methylendioxybenzyl)-1,2,3,4-tetrahydro-6-methoxyisoquinoline

: 7687-01-6
2-benzyloxy-5,6,12,12a-tetrahydro-3-methoxy-9,10-methylenedioxybenz[b,g]indolizine

Guidance literature:: With sodium t-butanolate; (IMes)2Pd(η3-allyl)Cl; In toluene; at 80 ℃; for 14h;
DOI:10.1055/s-2003-41468

Reference yield: 90.0%

: 7687-02-7
2-benzyloxy-3-methoxy-9,10-(methylenedioxy)-5,6-dihydroindolo[2,1-a]isoquinoline

: 7687-01-6
2-benzyloxy-5,6,12,12a-tetrahydro-3-methoxy-9,10-methylenedioxybenz[b,g]indolizine

Guidance literature:: With sodium cyanoborohydride; In acetic acid;
DOI:10.1021/ol005802d

Reference yield:

: 7686-98-8
7-benzyloxy-1-(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-6-methoxy-3,4-dihydro-isoquinoline

: 7687-01-6
2-benzyloxy-5,6,12,12a-tetrahydro-3-methoxy-9,10-methylenedioxybenz[b,g]indolizine

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / K₂CO₃ / dimethylformamide / 72 h / Heating

2: 90 percent / NaBH₃CN / acetic acid

With sodium cyanoborohydride; potassium carbonate; In acetic acid; N,N-dimethyl-formamide; 1: Cyclization / 2: Reduction;
DOI:10.1021/ol005802d