N¹,N⁴-bis((E)-1-cyclohexylaminocarbonyl-2-hydroxy-2-phenylethenyl)-N¹,N⁴-bis(2-nitrobenzyl)terephthalamide

Base Information

• Chemical Name: N¹,N⁴-bis((E)-1-cyclohexylaminocarbonyl-2-hydroxy-2-phenylethenyl)-N¹,N⁴-bis(2-nitrobenzyl)terephthalamide
• CAS No.: 1631151-78-4
• Molecular Formula: C₅₂H₅₂N₆O₁₀
• Molecular Weight: 921.019

Synonyms:N¹,N⁴-bis((E)-1-cyclohexylaminocarbonyl-2-hydroxy-2-phenylethenyl)-N¹,N⁴-bis(2-nitrobenzyl)terephthalamide

Chemical Property of N¹,N⁴-bis((E)-1-cyclohexylaminocarbonyl-2-hydroxy-2-phenylethenyl)-N¹,N⁴-bis(2-nitrobenzyl)terephthalamide

Chemical Property:

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Technology Process of N¹,N⁴-bis((E)-1-cyclohexylaminocarbonyl-2-hydroxy-2-phenylethenyl)-N¹,N⁴-bis(2-nitrobenzyl)terephthalamide

There total 1 articles about N¹,N⁴-bis((E)-1-cyclohexylaminocarbonyl-2-hydroxy-2-phenylethenyl)-N¹,N⁴-bis(2-nitrobenzyl)terephthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

Cyclohexyl isocyanide (931-53-3) + phenylglyoxal hydrate (1074-12-0) + terephthalic acid (100-21-0) + 2-nitrobenzylamine hydrochloride (24835-08-3) → N1,N4-bis((E)-1-cyclohexylaminocarbonyl-2-hydroxy-2-phenylethenyl)-N1,N4-bis(2-nitrobenzyl)terephthalamide (1631151-78-4)

Guidance literature:

2-nitrobenzylamine hydrochloride; With potassium hydroxide; for 0.166667h;

phenylglyoxal hydrate; at 20 ℃; for 0.25h;

Cyclohexyl isocyanide; terephthalic acid; at 20 ℃; for 48h;

DOI:10.1039/c4ob00444b

Reference yield: 87.0%

N1,N4-bis((E)-1-cyclohexylaminocarbonyl-2-hydroxy-2-phenylethenyl)-N1,N4-bis(2-nitrobenzyl)terephthalamide (1631151-78-4) → 4,4'-terephthaloyl bis(N-cyclohexyl-2-phenyl-4,5-dihydro-1H-benzo[e][1,4]diazepine-3-carboxamide) (1616367-17-9)

Guidance literature:

With hydrogenchloride; tin(ll) chloride; In ethanol; for 0.75h; Reflux;

DOI:10.1039/c4ob00444b

upstream raw materials:

Cyclohexyl isocyanide

phenylglyoxal hydrate

terephthalic acid

2-nitrobenzylamine hydrochloride

Downstream raw materials:

4,4'-terephthaloyl bis(N-cyclohexyl-2-phenyl-4,5-dihydro-1H-benzo[e][1,4]diazepine-3-carboxamide)

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