6,6-diphenyl-1,3-bis-trimethylsilanyl-4H,8H-5,7-dioxa-6-sila-azulen-2-one

Base Information

Chemical Name:6,6-diphenyl-1,3-bis-trimethylsilanyl-4H,8H-5,7-dioxa-6-sila-azulen-2-one
CAS No.:462660-30-6
Molecular Formula:C₂₅H₃₂O₃Si₃
Molecular Weight:464.784
Hs Code.:

6,6-diphenyl-1,3-bis-trimethylsilanyl-4<i>H</i>,8<i>H</i>-5,7-dioxa-6-sila-azulen-2-one

Synonyms:6,6-diphenyl-1,3-bis-trimethylsilanyl-4H,8H-5,7-dioxa-6-sila-azulen-2-one

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Chemical Property of 6,6-diphenyl-1,3-bis-trimethylsilanyl-4H,8H-5,7-dioxa-6-sila-azulen-2-one

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Technology Process of 6,6-diphenyl-1,3-bis-trimethylsilanyl-4H,8H-5,7-dioxa-6-sila-azulen-2-one

There total 3 articles about 6,6-diphenyl-1,3-bis-trimethylsilanyl-4H,8H-5,7-dioxa-6-sila-azulen-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 201230-82-2
carbon monoxide

: 462660-29-3
C₂₄H₃₂O₂Si₃

: 462660-31-7
2,5-bis(trimethylsilyl)-3,4-bis(hydroxymethyl)cyclopentadienone

: 462660-30-6
6,6-diphenyl-1,3-bis-trimethylsilanyl-4H,8H-5,7-dioxa-6-sila-azulen-2-one

Guidance literature:: carbon monoxide; C₂₄H₃₂O₂Si₃; iron pentacarbonyl; In toluene; at 120 ℃; for 24h; under 3102.97 Torr;

With trimethylamine-N-oxide; In acetone; at 0 ℃; for 4h; Further stages.;
DOI:10.1021/ol020099+

Reference yield:

: 5272-36-6
3-trimethylsilyl-2-propyn-1-ol

: 462660-30-6
6,6-diphenyl-1,3-bis-trimethylsilanyl-4H,8H-5,7-dioxa-6-sila-azulen-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: 82 percent / 2,6-lutidine / CH₂Cl₂ / 4 h / 0 - 23 °C

2.1: Fe(CO)5 / toluene / 24 h / 120 °C / 3102.97 Torr

2.2: Me₃NO / acetone / 4 h / 0 °C

With 2,6-dimethylpyridine; iron pentacarbonyl; In dichloromethane; toluene;
DOI:10.1021/ol020099+

Reference yield:

: 80-10-4
diphenylsilyl dichloride

: 462660-30-6
6,6-diphenyl-1,3-bis-trimethylsilanyl-4H,8H-5,7-dioxa-6-sila-azulen-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: 82 percent / 2,6-lutidine / CH₂Cl₂ / 4 h / 0 - 23 °C

2.1: Fe(CO)5 / toluene / 24 h / 120 °C / 3102.97 Torr

2.2: Me₃NO / acetone / 4 h / 0 °C

With 2,6-dimethylpyridine; iron pentacarbonyl; In dichloromethane; toluene;
DOI:10.1021/ol020099+