methanesulfonic acid 3-(diisopropyloxy-phosphorylmethoxy)-1-trityloxymethyl-propyl ester

Base Information

Chemical Name:methanesulfonic acid 3-(diisopropyloxy-phosphorylmethoxy)-1-trityloxymethyl-propyl ester
CAS No.:918795-62-7
Molecular Formula:C₃₁H₄₁O₈PS
Molecular Weight:604.701
Hs Code.:

Synonyms:methanesulfonic acid 3-(diisopropyloxy-phosphorylmethoxy)-1-trityloxymethyl-propyl ester

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Chemical Property of methanesulfonic acid 3-(diisopropyloxy-phosphorylmethoxy)-1-trityloxymethyl-propyl ester

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Technology Process of methanesulfonic acid 3-(diisopropyloxy-phosphorylmethoxy)-1-trityloxymethyl-propyl ester

There total 3 articles about methanesulfonic acid 3-(diisopropyloxy-phosphorylmethoxy)-1-trityloxymethyl-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 918795-60-5
[3-hydroxy-4-trityloxy-butoxymethyl]-phosphonic acid diisopropyl ester

: 124-63-0
methanesulfonyl chloride

: 918795-62-7
methanesulfonic acid 3-(diisopropyloxy-phosphorylmethoxy)-1-trityloxymethyl-propyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1080/15257770500446816

Reference yield:

: 918795-56-9
[2-(2,2-dimethyl[1,3]dioxolan-4-yl)ethoxymethyl]-phosphonic acid diisopropyl ester

: 918795-62-7
methanesulfonic acid 3-(diisopropyloxy-phosphorylmethoxy)-1-trityloxymethyl-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 36 percent / acetic acid / 16 h / 20 °C

2: 75 percent / pyridine; DMAP / 48 h / 20 °C

3: 84 percent / triethylamine; DMAP / CH₂Cl₂ / 16 h / 20 °C

With pyridine; dmap; acetic acid; triethylamine; In dichloromethane;
DOI:10.1080/15257770500446816

Reference yield:

: 35717-98-7
bis(2-propyl)-p-toluenesulfonyloxymethylphosphonate

: 918795-62-7
methanesulfonic acid 3-(diisopropyloxy-phosphorylmethoxy)-1-trityloxymethyl-propyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 59 percent / dimethylformamide / 16 h / 20 °C

2: 36 percent / acetic acid / 16 h / 20 °C

3: 75 percent / pyridine; DMAP / 48 h / 20 °C

4: 84 percent / triethylamine; DMAP / CH₂Cl₂ / 16 h / 20 °C

With pyridine; dmap; acetic acid; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/15257770500446816