2-[((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butylcarbamoyl)-methyl]-benzoic acid

Base Information

Chemical Name:2-[((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butylcarbamoyl)-methyl]-benzoic acid
CAS No.:185825-41-6
Molecular Formula:C₂₃H₂₆N₂O₇
Molecular Weight:442.469
Hs Code.:

Synonyms:2-[((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butylcarbamoyl)-methyl]-benzoic acid

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Chemical Property of 2-[((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butylcarbamoyl)-methyl]-benzoic acid

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Technology Process of 2-[((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butylcarbamoyl)-methyl]-benzoic acid

There total 1 articles about 2-[((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butylcarbamoyl)-methyl]-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 137559-30-9
methyl N^α-(benzyloxycarbonyl)-L-ornithinate

: 703-59-3
homophthalic anhydride

: 185825-41-6
2-[((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butylcarbamoyl)-methyl]-benzoic acid

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In ethanol; for 6h; Heating;
DOI:10.1021/jm9606453

Reference yield: 95.0%

: 67-56-1
methanol

: 185825-41-6
2-[((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butylcarbamoyl)-methyl]-benzoic acid

: 185825-43-8
2-[((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butylcarbamoyl)-methyl]-benzoic acid methyl ester

Guidance literature:: With thionyl chloride; for 18h; Ambient temperature;
DOI:10.1021/jm9606453

Reference yield:

: 185825-41-6
2-[((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butylcarbamoyl)-methyl]-benzoic acid

: 2-[((S)-4-Amino-4-methoxycarbonyl-butylcarbamoyl)-methyl]-benzoic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / SOCl₂ / 18 h / Ambient temperature

2: 44 percent / H₂, 6 N HCl, glacial AcOH / 10percent Pd/C / ethanol / 14 h / 1551.4 Torr

With hydrogenchloride; thionyl chloride; hydrogen; acetic acid; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm9606453