4-bromo-3-iodobenzonitrile

Base Information

• Chemical Name: 4-bromo-3-iodobenzonitrile
• CAS No.: 1006715-27-0
• Molecular Formula: C₇H₃BrIN
• Molecular Weight: 307.916
• Hs Code.: 2926907090
• Mol file: 1006715-27-0.mol

Synonyms:4-bromo-3-iodobenzonitrile

Chemical Property of 4-bromo-3-iodobenzonitrile

Chemical Property:

• Boiling Point: 307.8±27.0 °C(Predicted)
• Density: 2.31±0.1 g/cm3(Predicted)
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature

Purity/Quality:

98% purity ^*data from raw suppliers

4-Bromo-3-iodobenzonitrile ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 4-bromo-3-iodobenzonitrile

There total 1 articles about 4-bromo-3-iodobenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bromobenzenecarbonitrile (623-00-7) → 4-bromo-2-iodobenzonitrile (944276-67-9) + 4-bromo-3-iodobenzonitrile (1006715-27-0)

Guidance literature:

4-bromobenzenecarbonitrile; In tetrahydrofuran; hexane; pentane; at -30 ℃; for 2h;

With iodine; In tetrahydrofuran; hexane; pentane; at 20 ℃; for 1h; Further stages.;

DOI:10.1021/ja071268u

Reference yield:

2-ethynylaniline (52670-38-9) + 4-bromo-3-iodobenzonitrile (1006715-27-0) → C15H9BrN2

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 20 ℃; Inert atmosphere;

DOI:10.1039/c6ob01029f

upstream raw materials:

4-bromobenzenecarbonitrile

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