3,7-dibenzyl-1,5-dimethyl-9-oxo-3,7-diazabicyclo<3.3.1>nonane

Base Information

• Chemical Name: 3,7-dibenzyl-1,5-dimethyl-9-oxo-3,7-diazabicyclo<3.3.1>nonane
• CAS No.: 107606-92-8
• Molecular Formula: C₂₃H₂₈N₂O
• Molecular Weight: 348.488
• Mol file: 107606-92-8.mol

Synonyms:3,7-dibenzyl-1,5-dimethyl-9-oxo-3,7-diazabicyclo<3.3.1>nonane

Chemical Property of 3,7-dibenzyl-1,5-dimethyl-9-oxo-3,7-diazabicyclo<3.3.1>nonane

Chemical Property:

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Technology Process of 3,7-dibenzyl-1,5-dimethyl-9-oxo-3,7-diazabicyclo<3.3.1>nonane

There total 4 articles about 3,7-dibenzyl-1,5-dimethyl-9-oxo-3,7-diazabicyclo<3.3.1>nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

benzyl bromide (100-39-0) + 1,5-dimethyl-9-oxo-3,7-diazabicyclo-<3.3.1>nonane (80808-96-4) → 3,7-dibenzyl-1,5-dimethyl-9-oxo-3,7-diazabicyclo<3.3.1>nonane (107606-92-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; for 10h; Reflux;

DOI:10.1021/acsmedchemlett.1c00299

Reference yield: 75.0%

benzyl chloride (100-44-7) + 2,2,5,7-tetramethyl-1,3-diazaadamantan-6-one (108790-76-7) → 3,7-dibenzyl-1,5-dimethyl-9-oxo-3,7-diazabicyclo<3.3.1>nonane (107606-92-8)

Guidance literature:

With triethylamine; In 1,4-dioxane; for 15h; Heating;

DOI:10.1007/BF00474490

Reference yield: 5.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + pentan-3-one (96-22-0) + benzylamine (100-46-9) → 3,7-dibenzyl-1,5-dimethyl-9-oxo-3,7-diazabicyclo<3.3.1>nonane (107606-92-8)

Guidance literature:

With acetic acid; In ethanol; for 5h; Heating;

DOI:10.1016/0040-4020(94)01069-C

upstream raw materials:

benzyl chloride

2,2,5,7-tetramethyl-1,3-diazaadamantan-6-one

formaldehyd

pentan-3-one

Downstream raw materials:

3,7-dibenzyl-1,5-dimethyl-9-hydroxy-3,7-diazabicyclo<3.3.1>nonane

(3,7-dibenzyl-1,5-dimethylbispidinone)(2-methylene-6,6-dimethylbicyclo[3.1.1]hept-2,3,10-enyl)palladium trifluoromethanesulfonate

(3,7-dibenzyl-1,5-dimethylbispidinone)(1,3-η(3)-propenyl)palladium trifluoromethanesulfonate

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