Mono<amino>succinyl>-N-(benzyloxy)amino>butyl> bis<butyl> isocyanurate

Base Information

Chemical Name:Mono<amino>succinyl>-N-(benzyloxy)amino>butyl> bis<butyl> isocyanurate
CAS No.:153756-43-5
Molecular Formula:C₅₉H₆₈ClN₉O₁₅
Molecular Weight:1178.69
Hs Code.:

Mono<<N-<<<1-carba-3-chloro-4-(p-nitrobenzyloxycarbonyl)-3-cephem-7-yl>amino>succinyl>-N-(benzyloxy)amino>butyl> bis<<N-acetyl-N-(benzyloxy)amino>butyl> isocyanurate

Synonyms:Mono<amino>succinyl>-N-(benzyloxy)amino>butyl> bis<butyl> isocyanurate

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Chemical Property of Mono<amino>succinyl>-N-(benzyloxy)amino>butyl> bis<butyl> isocyanurate

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Technology Process of Mono<amino>succinyl>-N-(benzyloxy)amino>butyl> bis<butyl> isocyanurate

There total 2 articles about Mono<amino>succinyl>-N-(benzyloxy)amino>butyl> bis<butyl> isocyanurate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.5%

: 123932-46-7
carbacephalosporin hydrochloride

: 153756-41-3
Mono<butyl> bis<butyl> isocyanurate

: 153756-43-5
Mono<amino>succinyl>-N-(benzyloxy)amino>butyl> bis<butyl> isocyanurate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; 1.) 0 deg C, 30 min, 2.) room temp., overnight;
DOI:10.1021/jo00084a018

Reference yield:

: 153756-40-2
Mono<-N-(benzyloxy)amino>butyl>bis<butyl> isocyanurate

: 153756-43-5
Mono<amino>succinyl>-N-(benzyloxy)amino>butyl> bis<butyl> isocyanurate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Zn, AcOH / tetrahydrofuran / Ambient temperature

2: 57.5 percent / N-hydroxybenzotriazole hydrate, 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride, triethylamine / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) room temp., overnight

With benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00084a018