3-(4-methoxy-phenyl)-N-{4-[3-(4-methoxy-phenyl)-acryloylamino]-butyl}-N-{3-[3-(4-methoxy-phenyl)-acryloylamino]-propyl}-acrylamide

Base Information

Chemical Name:3-(4-methoxy-phenyl)-N-{4-[3-(4-methoxy-phenyl)-acryloylamino]-butyl}-N-{3-[3-(4-methoxy-phenyl)-acryloylamino]-propyl}-acrylamide
CAS No.:131086-79-8
Molecular Formula:C₃₇H₄₃N₃O₆
Molecular Weight:625.765
Hs Code.:

3-(4-methoxy-phenyl)-<i>N</i>-{4-[3-(4-methoxy-phenyl)-acryloylamino]-butyl}-<i>N</i>-{3-[3-(4-methoxy-phenyl)-acryloylamino]-propyl}-acrylamide

Synonyms:3-(4-methoxy-phenyl)-N-{4-[3-(4-methoxy-phenyl)-acryloylamino]-butyl}-N-{3-[3-(4-methoxy-phenyl)-acryloylamino]-propyl}-acrylamide

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Chemical Property of 3-(4-methoxy-phenyl)-N-{4-[3-(4-methoxy-phenyl)-acryloylamino]-butyl}-N-{3-[3-(4-methoxy-phenyl)-acryloylamino]-propyl}-acrylamide

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Technology Process of 3-(4-methoxy-phenyl)-N-{4-[3-(4-methoxy-phenyl)-acryloylamino]-butyl}-N-{3-[3-(4-methoxy-phenyl)-acryloylamino]-propyl}-acrylamide

There total 6 articles about 3-(4-methoxy-phenyl)-N-{4-[3-(4-methoxy-phenyl)-acryloylamino]-butyl}-N-{3-[3-(4-methoxy-phenyl)-acryloylamino]-propyl}-acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 34446-64-5,42996-84-9
(E)-3-(4-methoxyphenyl)propenoyl chloride

: 334-50-9,35408-56-1
spermidine trihydrochloride

: 131086-79-8
3-(4-methoxy-phenyl)-N-{4-[3-(4-methoxy-phenyl)-acryloylamino]-butyl}-N-{3-[3-(4-methoxy-phenyl)-acryloylamino]-propyl}-acrylamide

Guidance literature:: With triethylamine; In ethyl acetate; at 25 ℃;
DOI:10.1016/S0040-4020(98)01014-X

Reference yield:

: 943-89-5
(E)-3-(4-methoxyphenyl)acrylic acid

: 131086-79-8
3-(4-methoxy-phenyl)-N-{4-[3-(4-methoxy-phenyl)-acryloylamino]-butyl}-N-{3-[3-(4-methoxy-phenyl)-acryloylamino]-propyl}-acrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / oxalyl chloride / toluene

2: 83 percent / Et₃N / ethyl acetate / 25 °C

With oxalyl dichloride; triethylamine; In ethyl acetate; toluene;
DOI:10.1016/S0040-4020(98)01014-X

Reference yield:

: 3-(3-chloro-propylamino)-propionitrile

: 131086-79-8
3-(4-methoxy-phenyl)-N-{4-[3-(4-methoxy-phenyl)-acryloylamino]-butyl}-N-{3-[3-(4-methoxy-phenyl)-acryloylamino]-propyl}-acrylamide

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / Et₃N / CH₂Cl₂ / 25 °C

2: 68 percent / NaI / aq. ethanol / Heating

3: 87 percent / NaOH, Raney-Ni, H₂ / ethanol; H₂O / 20 h / 25 °C / 2068.59 Torr

4: HCl / H₂O / 25 °C

5: 83 percent / Et₃N / ethyl acetate / 25 °C

With hydrogenchloride; sodium hydroxide; hydrogen; nickel; triethylamine; sodium iodide; In ethanol; dichloromethane; water; ethyl acetate;
DOI:10.1016/S0040-4020(98)01014-X