3-(2-nitro-3-piperidin-1-yl-phenyl)-2,5-dioxo-hexanedioic acid diethyl ester

Base Information

Chemical Name:3-(2-nitro-3-piperidin-1-yl-phenyl)-2,5-dioxo-hexanedioic acid diethyl ester
CAS No.:1057292-51-9
Molecular Formula:C₂₁H₂₆N₂O₈
Molecular Weight:434.446
Hs Code.:

Synonyms:3-(2-nitro-3-piperidin-1-yl-phenyl)-2,5-dioxo-hexanedioic acid diethyl ester

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Chemical Property of 3-(2-nitro-3-piperidin-1-yl-phenyl)-2,5-dioxo-hexanedioic acid diethyl ester

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Technology Process of 3-(2-nitro-3-piperidin-1-yl-phenyl)-2,5-dioxo-hexanedioic acid diethyl ester

There total 4 articles about 3-(2-nitro-3-piperidin-1-yl-phenyl)-2,5-dioxo-hexanedioic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1057292-55-3
3-(2-nitro-3-piperidin-1-yl-phenyl)-2-oxo-propionic acid ethyl ester

: 70-23-5
ethyl Bromopyruvate

: 1057292-51-9
3-(2-nitro-3-piperidin-1-yl-phenyl)-2,5-dioxo-hexanedioic acid diethyl ester

Guidance literature:: With potassium ethoxide; In tetrahydrofuran; at 0 - 20 ℃; for 1.5h;

Reference yield:

: 110-89-4
piperidine

: 1057292-51-9
3-(2-nitro-3-piperidin-1-yl-phenyl)-2,5-dioxo-hexanedioic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: C₁₁H₁₄NOPol / 1,4-dioxane / 56 h / Heating / reflux

2.1: lithium diisopropyl amide / tetrahydrofuran / 1.5 h / 0 - 20 °C

2.2: 20 °C

3.1: potassium ethoxide / tetrahydrofuran / 1.5 h / 0 - 20 °C

With C₁₁H₁₄NOPol; potassium ethoxide; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 52414-97-8
1-bromo-3-methyl-2-nitro-benzene

: 1057292-51-9
3-(2-nitro-3-piperidin-1-yl-phenyl)-2,5-dioxo-hexanedioic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: C₁₁H₁₄NOPol / 1,4-dioxane / 56 h / Heating / reflux

2.1: lithium diisopropyl amide / tetrahydrofuran / 1.5 h / 0 - 20 °C

2.2: 20 °C

3.1: potassium ethoxide / tetrahydrofuran / 1.5 h / 0 - 20 °C

With C₁₁H₁₄NOPol; potassium ethoxide; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane;