Technology Process of dimethyl 2-methyl-2-(3'-benzoyl)phenylpropanedioate
There total 6 articles about dimethyl 2-methyl-2-(3'-benzoyl)phenylpropanedioate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 97 percent / SnCl2*2H2O / ethyl acetate / 1 h / Heating
2: 1) NaNO2, HCl, 2) NaOAc / 2) EtOH, 0 deg C, 30 min
3: 38 percent / t-BuOK / dimethylsulfoxide / Irradiation
4: 80 percent / t-BuOK / tetrahydrofuran / 0.5 h / 25 °C
With
hydrogenchloride; potassium tert-butylate; sodium acetate; tin(ll) chloride; sodium nitrite;
In
tetrahydrofuran; dimethyl sulfoxide; ethyl acetate;
DOI:10.1016/S0040-4020(01)85294-7
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) NaNO2, HCl, 2) NaOAc / 2) EtOH, 0 deg C, 30 min
2: 38 percent / t-BuOK / dimethylsulfoxide / Irradiation
3: 80 percent / t-BuOK / tetrahydrofuran / 0.5 h / 25 °C
With
hydrogenchloride; potassium tert-butylate; sodium acetate; sodium nitrite;
In
tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1016/S0040-4020(01)85294-7
