(E)-3-(3-Cyclopentyloxy-4-methoxy-phenyl)-N-methoxy-2,N-dimethyl-acrylamide

Base Information

Chemical Name:(E)-3-(3-Cyclopentyloxy-4-methoxy-phenyl)-N-methoxy-2,N-dimethyl-acrylamide
CAS No.:168170-00-1
Molecular Formula:C₁₈H₂₅NO₄
Molecular Weight:319.401
Hs Code.:

Synonyms:(E)-3-(3-Cyclopentyloxy-4-methoxy-phenyl)-N-methoxy-2,N-dimethyl-acrylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(3-Cyclopentyloxy-4-methoxy-phenyl)-N-methoxy-2,N-dimethyl-acrylamide

Chemical Property:

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Technology Process of (E)-3-(3-Cyclopentyloxy-4-methoxy-phenyl)-N-methoxy-2,N-dimethyl-acrylamide

There total 5 articles about (E)-3-(3-Cyclopentyloxy-4-methoxy-phenyl)-N-methoxy-2,N-dimethyl-acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 168169-98-0
(E)-3-<3-(cyclopentyloxy)-4-methoxyphenyl>-2-methylpropionic acid

: 168170-00-1
(E)-3-(3-Cyclopentyloxy-4-methoxy-phenyl)-N-methoxy-2,N-dimethyl-acrylamide

Guidance literature:: With 1,1'-carbonyldiimidazole;

Reference yield:

: 621-59-0
isovanillin

: 168170-00-1
(E)-3-(3-Cyclopentyloxy-4-methoxy-phenyl)-N-methoxy-2,N-dimethyl-acrylamide

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / dimethylformamide

2: LHMDS / tetrahydrofuran

3: LiOH / dioxane; H₂O

4: 82 percent / CDI

With lithium hydroxide; potassium carbonate; 1,1'-carbonyldiimidazole; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;

Reference yield:

: 137-43-9
Cyclopentyl bromide

: 168170-00-1
(E)-3-(3-Cyclopentyloxy-4-methoxy-phenyl)-N-methoxy-2,N-dimethyl-acrylamide

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / dimethylformamide

2: LHMDS / tetrahydrofuran

3: LiOH / dioxane; H₂O

4: 82 percent / CDI

With lithium hydroxide; potassium carbonate; 1,1'-carbonyldiimidazole; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;