5-phenyl-2-(pyridin-3-yl)-4,5-dihydrothiazole

Base Information

Chemical Name:5-phenyl-2-(pyridin-3-yl)-4,5-dihydrothiazole
CAS No.:1062214-34-9
Molecular Formula:C₁₄H₁₂N₂S
Molecular Weight:240.329
Hs Code.:

Synonyms:5-phenyl-2-(pyridin-3-yl)-4,5-dihydrothiazole

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Chemical Property of 5-phenyl-2-(pyridin-3-yl)-4,5-dihydrothiazole

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Technology Process of 5-phenyl-2-(pyridin-3-yl)-4,5-dihydrothiazole

There total 3 articles about 5-phenyl-2-(pyridin-3-yl)-4,5-dihydrothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 59-67-6
nicotinic acid

: 7568-93-6,1936-63-6
2-Amino-1-phenylethanol

: 106950-01-0
5-phenyl-2-(pyridin-3-yl)thiazole

: 1062214-34-9
5-phenyl-2-(pyridin-3-yl)-4,5-dihydrothiazole

Guidance literature:: With Lawessons reagent; at 150 ℃; for 0.133333h; microwave irradiation;
DOI:10.1016/j.tet.2008.07.027

Reference yield:

: 4621-66-3
thionicotinamide

: 102921-26-6,93-52-7
(1,2-dibromoethyl)benzene

: 1062214-34-9
5-phenyl-2-(pyridin-3-yl)-4,5-dihydrothiazole

Guidance literature:: With sodium hydrogencarbonate; In acetonitrile; at 80 ℃; for 15h;
DOI:10.1021/acs.orglett.7b00079

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1062214-34-9
5-phenyl-2-(pyridin-3-yl)-4,5-dihydrothiazole

Guidance literature:: Multi-step reaction with 2 steps

1: urea hydrogen peroxide adduct; lithium bromide; trifluoroacetic acid / acetonitrile / 1 h / 80 °C

2: sodium hydrogencarbonate / acetonitrile / 15 h / 80 °C

With urea hydrogen peroxide adduct; sodium hydrogencarbonate; trifluoroacetic acid; lithium bromide; In acetonitrile;
DOI:10.1021/acs.orglett.7b00079