Benzaldehyde (5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

Base Information

Chemical Name:Benzaldehyde (5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone
CAS No.:97693-29-3
Molecular Formula:C₁₈H₁₃N₅O
Molecular Weight:315.334
Hs Code.:

Synonyms:Benzaldehyde (5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

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Chemical Property of Benzaldehyde (5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

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Technology Process of Benzaldehyde (5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

There total 6 articles about Benzaldehyde (5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 97693-25-9
5-cyano-2-hydrazino-6-phenyl-4-oxopyrimidine

: 100-52-7
benzaldehyde

: 97693-29-3
Benzaldehyde (5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

Guidance literature:: In ethanol; for 2h; Heating;

Reference yield: 75.0%

: 100-52-7
benzaldehyde

: 97693-25-9
5-cyano-2-hydrazono-6-phenyl-1,2,3,4-tetrahydro pyrimidin-4-one

: 97693-29-3
4-Oxo-6-phenyl-2-{[1-phenyl-meth-(E)-ylidene]-hydrazono}-1,2,3,4-tetrahydro-pyrimidine-5-carbonitrile

Guidance literature:: In acetic acid; for 1h; Heating;

Reference yield:

: 2025-40-3
ethyl benzylidenecyanoacetate

: 97693-29-3
Benzaldehyde (5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate / pyridine / Heating

2: 75 percent / hydrazine hydrate / ethanol / 2 h / Heating

3: 81 percent / ethanol / 2 h / Heating

With sodium acetate; hydrazine hydrate; In pyridine; ethanol;