1-methyl-5-(3-methyl-4-nitrobenzoyl)-1,4,5,10-tetrahydropyrazolo[3,4-b][1,5]benzodiazepine

Base Information

Chemical Name:1-methyl-5-(3-methyl-4-nitrobenzoyl)-1,4,5,10-tetrahydropyrazolo[3,4-b][1,5]benzodiazepine
CAS No.:1209963-09-6
Molecular Formula:C₁₉H₁₇N₅O₃
Molecular Weight:363.376
Hs Code.:

Synonyms:1-methyl-5-(3-methyl-4-nitrobenzoyl)-1,4,5,10-tetrahydropyrazolo[3,4-b][1,5]benzodiazepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-methyl-5-(3-methyl-4-nitrobenzoyl)-1,4,5,10-tetrahydropyrazolo[3,4-b][1,5]benzodiazepine

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Technology Process of 1-methyl-5-(3-methyl-4-nitrobenzoyl)-1,4,5,10-tetrahydropyrazolo[3,4-b][1,5]benzodiazepine

There total 1 articles about 1-methyl-5-(3-methyl-4-nitrobenzoyl)-1,4,5,10-tetrahydropyrazolo[3,4-b][1,5]benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35675-46-8
3-methyl-4-nitro-benzoyl chloride

: 479234-83-8
1-methyl-1,4,5,10-tetrahydrobenzo[b]pyrazolo[3,4-e][1,4]diazepine

: 1209963-09-6
1-methyl-5-(3-methyl-4-nitrobenzoyl)-1,4,5,10-tetrahydropyrazolo[3,4-b][1,5]benzodiazepine

Guidance literature:: With N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm901084f

Reference yield: 82.0%

: 1209963-09-6
1-methyl-5-(3-methyl-4-nitrobenzoyl)-1,4,5,10-tetrahydropyrazolo[3,4-b][1,5]benzodiazepine

: 1209963-10-9
2-methyl-4-[(1-methyl-4,10-dihydropyrazolo[3,4-b][1,5]benzodiazepin-5(1H)-yl)carbonyl]aniline

Guidance literature:: 1-methyl-5-(3-methyl-4-nitrobenzoyl)-1,4,5,10-tetrahydropyrazolo[3,4-b][1,5]benzodiazepine; With tin(II) chloride dihdyrate; In ethanol; for 1h; Reflux; Inert atmosphere;

With sodium hydrogencarbonate; In ethanol; water; at 0 - 20 ℃; pH=7 - 8;
DOI:10.1021/jm901084f