5-cyano-1,6-dihydro-4-methyl-1-p-tolyl-6-oxopyridazine-3-carboxylic acid hydrazide

Base Information

• Chemical Name: 5-cyano-1,6-dihydro-4-methyl-1-p-tolyl-6-oxopyridazine-3-carboxylic acid hydrazide
• CAS No.: 144362-55-0
• Molecular Formula: C₁₄H₁₃N₅O₂
• Molecular Weight: 283.29

Synonyms:5-cyano-1,6-dihydro-4-methyl-1-p-tolyl-6-oxopyridazine-3-carboxylic acid hydrazide

Chemical Property of 5-cyano-1,6-dihydro-4-methyl-1-p-tolyl-6-oxopyridazine-3-carboxylic acid hydrazide

Chemical Property:

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Technology Process of 5-cyano-1,6-dihydro-4-methyl-1-p-tolyl-6-oxopyridazine-3-carboxylic acid hydrazide

There total 1 articles about 5-cyano-1,6-dihydro-4-methyl-1-p-tolyl-6-oxopyridazine-3-carboxylic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ethyl-5-cyano-1,6-dihydro-4-methyl-6-oxo-1-(4-tolyl)-3-pyridazinecarboxylate (125040-80-4) → 5-cyano-1,6-dihydro-4-methyl-1-p-tolyl-6-oxopyridazine-3-carboxylic acid hydrazide (144362-55-0)

Guidance literature:

With hydrazine hydrate; In ethanol; for 2h; Heating;

DOI:10.1002/prac.19923340816

Reference yield: 85.0%

5-cyano-1,6-dihydro-4-methyl-1-p-tolyl-6-oxopyridazine-3-carboxylic acid hydrazide (144362-55-0) → 5-amino-3,4-dihydro-3-p-tolylthieno<3,4-d>-pyridazin-1-carboxylic acid hydrazide (144362-60-7)

Guidance literature:

With piperidine; sulfur; In ethanol; for 2h; Heating;

DOI:10.1002/prac.19923340816

Reference yield: 85.0%

benzaldehyde (100-52-7) + 5-cyano-1,6-dihydro-4-methyl-1-p-tolyl-6-oxopyridazine-3-carboxylic acid hydrazide (144362-55-0) → 7-benzylidenamido-2,3,7,8-tetrahydro-3-oxo-2-p-tolyl-6-phenylpyrido<3,4-c>-pyridazin-3-carbonitrile

Guidance literature:

With piperidine; In ethanol; for 1h; Heating;

DOI:10.1002/prac.19923340816

upstream raw materials:

ethyl-5-cyano-1,6-dihydro-4-methyl-6-oxo-1-(4-tolyl)-3-pyridazinecarboxylate

Downstream raw materials:

N-benzylidene-5-cyano-1,6-dihydro-4-methyl-6-oxo-1-p-tolylpyridazine-3-hydrazide

5-amino-3,4-dihydro-3-p-tolylthieno<3,4-d>-pyridazin-1-carboxylic acid hydrazide

5-Cyano-4-methyl-6-oxo-1-p-tolyl-1,6-dihydro-pyridazine-3-carbonyl azide

N-benzylidene 5-amino-3,4-dihydro-3-p-tolylthieno<3,4-d>pyridazin-1-hydrazide

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