ethyl {[4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}acetate

Base Information

Chemical Name:ethyl {[4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}acetate
CAS No.:74271-11-7
Molecular Formula:C₁₇H₁₅ClN₄O₂S
Molecular Weight:374.851
Hs Code.:

Synonyms:ethyl {[4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}acetate

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Chemical Property of ethyl {[4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}acetate

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Technology Process of ethyl {[4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}acetate

There total 5 articles about ethyl {[4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.6%

: 74270-76-1
4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazole-3-thiol

: 105-39-5
chloroacetic acid ethyl ester

: 74271-11-7
ethyl {[4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}acetate

Guidance literature:: 4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazole-3-thiol; With potassium hydroxide; In ethanol; for 0.5h; Reflux;

chloroacetic acid ethyl ester; In ethanol; Inert atmosphere;
DOI:10.2174/1570180815666180810122226

Reference yield:

: 74270-72-7
N-(4-chlorophenyl)-2-(pyridin-4-ylcarbonyl)hydrazinecarbothioamide

: 74271-11-7
ethyl {[4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / Reflux

2.1: potassium hydroxide / ethanol / 0.5 h / Reflux

2.2: Inert atmosphere

With potassium hydroxide; sodium hydroxide; In ethanol;
DOI:10.2174/1570180815666180810122226

Reference yield:

: 54-85-3,7640-37-1
isoniazid

: 74271-11-7
ethyl {[4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: Reflux

2.1: sodium hydroxide / Reflux

3.1: potassium hydroxide / ethanol / 0.5 h / Reflux

3.2: Inert atmosphere

With potassium hydroxide; sodium hydroxide; In ethanol;
DOI:10.2174/1570180815666180810122226