methyl 6-O-benzoyl-3,4-O-isopropylidene-2-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside

Base Information

• Chemical Name: methyl 6-O-benzoyl-3,4-O-isopropylidene-2-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside
• CAS No.: 124314-34-7
• Molecular Formula: C₂₁H₂₄N₂O₇S
• Molecular Weight: 448.497

Synonyms:methyl 6-O-benzoyl-3,4-O-isopropylidene-2-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside

Chemical Property of methyl 6-O-benzoyl-3,4-O-isopropylidene-2-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 6-O-benzoyl-3,4-O-isopropylidene-2-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside

There total 3 articles about methyl 6-O-benzoyl-3,4-O-isopropylidene-2-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoyl chloride (98-88-4) → methyl 6-O-benzoyl-3,4-O-isopropylidene-2-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside (124314-34-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / pyridine / CH₂Cl₂ / 0.25 h / -10 °C

2: 1.) toluene, reflux, 3 h; 2.) toluene, reflux, 1 h

With pyridine; In dichloromethane;

DOI:10.1016/0008-6215(89)84076-5

Reference yield:

methyl 3,4-di-O-isopropylidene-β-D-galactopyranoside (14897-47-3) → methyl 6-O-benzoyl-3,4-O-isopropylidene-2-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside (124314-34-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / pyridine / CH₂Cl₂ / 0.25 h / -10 °C

2: 1.) toluene, reflux, 3 h; 2.) toluene, reflux, 1 h

With pyridine; In dichloromethane;

DOI:10.1016/0008-6215(89)84076-5

Reference yield:

methyl 6-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside (71731-77-6) + 1,1'-Thiocarbonyldiimidazole (6160-65-2) → methyl 6-O-benzoyl-3,4-O-isopropylidene-2-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside (124314-34-7)

Guidance literature:

Yield given. Multistep reaction; 1.) toluene, reflux, 3 h; 2.) toluene, reflux, 1 h;

DOI:10.1016/0008-6215(89)84076-5

upstream raw materials:

methyl 6-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside

1,1'-Thiocarbonyldiimidazole

benzoyl chloride

methyl 3,4-di-O-isopropylidene-β-D-galactopyranoside

Downstream raw materials:

methyl 6-O-benzoyl-2-deoxy-β-D-lyxo-hexopyranoside

methyl 6-O-benzoyl-2-deoxy-3,4-O-isopropylidene-β-D-lyxo-hexopyranoside

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 124314-34-7 methyl 6-O-benzoyl-3,4-O-isopropylidene-2-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send