C₂₅H₂₂N₂O₆S₂

Base Information

Chemical Name:C₂₅H₂₂N₂O₆S₂
CAS No.:1313405-04-7
Molecular Formula:C₂₅H₂₂N₂O₆S₂
Molecular Weight:510.591
Hs Code.:

C<sub>25</sub>H<sub>22</sub>N<sub>2</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₂₅H₂₂N₂O₆S₂

Suppliers and Price of C₂₅H₂₂N₂O₆S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₂N₂O₆S₂

Chemical Property:

Purity/Quality:

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Technology Process of C₂₅H₂₂N₂O₆S₂

There total 5 articles about C₂₅H₂₂N₂O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313405-03-6
C₂₂H₁₉NO₇

: 96-53-7
2-mercaptothiazoline

: 1313405-04-7
C₂₅H₂₂N₂O₆S₂

Guidance literature:: C₂₂H₁₉NO₇; With thionyl chloride; N,N-dimethyl-formamide; In 1,4-dioxane; Reflux;

2-mercaptothiazoline; With triethylamine; In tetrahydrofuran; Cooling in ice;

Reference yield:

: 170235-19-5
methyl 2-bromo-3-hydroxy-6-pyridinecarboxylate

: 1313405-04-7
C₂₅H₂₂N₂O₆S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / acetonitrile / Reflux

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

3.1: potassium hydroxide; water / tetrahydrofuran / 80 °C

3.2: pH 2 / Cooling in ice

4.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 °C

5.1: potassium hydroxide; water / tetrahydrofuran / 20 °C

5.2: pH 2 / Cooling in ice

6.1: thionyl chloride / N,N-dimethyl-formamide / 1,4-dioxane / Reflux

6.2: Cooling in ice

With thionyl chloride; water; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1313404-99-7
methyl 2-bromo-3-[(ethylacetyl)oxy]-6-pyridinecarboxylate

: 1313405-04-7
C₂₅H₂₂N₂O₆S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

2.1: potassium hydroxide; water / tetrahydrofuran / 80 °C

2.2: pH 2 / Cooling in ice

3.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 °C

4.1: potassium hydroxide; water / tetrahydrofuran / 20 °C

4.2: pH 2 / Cooling in ice

5.1: thionyl chloride / N,N-dimethyl-formamide / 1,4-dioxane / Reflux

5.2: Cooling in ice

With thionyl chloride; water; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;