5-METHOXY-2-METHYL-4-NITROANILINE, TECH., 95

Base Information

• Chemical Name: 5-METHOXY-2-METHYL-4-NITROANILINE, TECH., 95
• CAS No.: 106579-00-4
• Molecular Formula: C8H10 N2 O3
• Molecular Weight: 182.179
• Hs Code.: 2922299090
• Mol file: 106579-00-4.mol

Synonyms:2-Methyl-5-(methyloxy)-4-nitroaniline;5-Methoxy-2-methyl-4-nitroaniline

Chemical Property of 5-METHOXY-2-METHYL-4-NITROANILINE, TECH., 95

Chemical Property:

• Vapor Pressure: 6.8E-06mmHg at 25°C
• Melting Point: 168-170 °C(lit.)
• Refractive Index: 1.589
• Boiling Point: 377.3°C at 760 mmHg
• Flash Point: 182°C
• PSA: 81.07000
• Density: 1.266g/cm³
• LogP: 2.59840
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

97% ^*data from raw suppliers

5-Methoxy-2-methyl-4-nitroaniline ^*data from reagent suppliers

Safty Information:

• Hazard Codes: F,Xn
• Statements: 11-20/21/22-36/37/38
• Safety Statements: 16-26-33-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-METHOXY-2-METHYL-4-NITROANILINE, TECH., 95

There total 3 articles about 5-METHOXY-2-METHYL-4-NITROANILINE, TECH., 95 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-methoxy-2-methyl-4-nitroacetanilide (361162-90-5) → 5-methoxy-2-methyl-4-nitroaniline (106579-00-4)

Guidance literature:

With sodium hydroxide;

Reference yield:

5’-methoxy-2’-methylacetanilide (50868-75-2) → 5-methoxy-2-methyl-4-nitroaniline (106579-00-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid; nitric acid / <3

2: aq. NaOH solution

With sodium hydroxide; sulfuric acid; nitric acid;

Reference yield:

5-chloro-2-methyl-4-nitroaniline (13852-51-2) + sodium methylate (124-41-4) → 5-methoxy-2-methyl-4-nitroaniline (106579-00-4)

Guidance literature:

at 130 ℃;

upstream raw materials:

5-chloro-2-methyl-4-nitroaniline

sodium methylate

5-methoxy-2-methyl-4-nitroacetanilide

5’-methoxy-2’-methylacetanilide

Downstream raw materials:

6-methoxy-5-nitro-1H-indazole

2-methyl-5-methoxy-1,4-phenylenediamine

5-methoxy-2-methyl-4-nitroacetanilide

1-fluoro-5-methoxy-2-methyl-4-nitro-benzene