N-((1-(3,6,9,12-tetraoxapentadec-14-ynyl)-1H-1,2,3-triazol-4-yl)bis(4-fluorophenyl)methoxy)phenyl

Base Information

Chemical Name:N-((1-(3,6,9,12-tetraoxapentadec-14-ynyl)-1H-1,2,3-triazol-4-yl)bis(4-fluorophenyl)methoxy)phenyl
CAS No.:1442461-47-3
Molecular Formula:C₃₂H₃₃F₂N₃O₅
Molecular Weight:577.628
Hs Code.:

Synonyms:N-((1-(3,6,9,12-tetraoxapentadec-14-ynyl)-1H-1,2,3-triazol-4-yl)bis(4-fluorophenyl)methoxy)phenyl

Suppliers and Price of N-((1-(3,6,9,12-tetraoxapentadec-14-ynyl)-1H-1,2,3-triazol-4-yl)bis(4-fluorophenyl)methoxy)phenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-((1-(3,6,9,12-tetraoxapentadec-14-ynyl)-1H-1,2,3-triazol-4-yl)bis(4-fluorophenyl)methoxy)phenyl

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-((1-(3,6,9,12-tetraoxapentadec-14-ynyl)-1H-1,2,3-triazol-4-yl)bis(4-fluorophenyl)methoxy)phenyl

There total 8 articles about N-((1-(3,6,9,12-tetraoxapentadec-14-ynyl)-1H-1,2,3-triazol-4-yl)bis(4-fluorophenyl)methoxy)phenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1416735-28-8
C₂₆H₂₈ClF₂N₃O₄

: 108-95-2,27073-41-2
phenol

: 1442461-47-3
N-((1-(3,6,9,12-tetraoxapentadec-14-ynyl)-1H-1,2,3-triazol-4-yl)bis(4-fluorophenyl)methoxy)phenyl

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; at 63 ℃; for 12h;

Reference yield:

: 1416735-20-0
2-(2-(2-(2-(4-(hydroxy)bis(4-fluorophenyl)-1H-1,2,3-triazol-1-yl)ethoxy)ethoxy)ethoxy)ethanol

: 1442461-47-3
N-((1-(3,6,9,12-tetraoxapentadec-14-ynyl)-1H-1,2,3-triazol-4-yl)bis(4-fluorophenyl)methoxy)phenyl

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 0 °C

1.2: 24 h / 20 °C

2.1: potassium hydrogensulfate / acetonitrile / 12 h / 20 °C

3.1: acetyl chloride / toluene / 100 °C

4.1: triethylamine; dmap / tetrahydrofuran / 12 h / 63 °C

With dmap; potassium hydrogensulfate; sodium hydride; triethylamine; acetyl chloride; In tetrahydrofuran; toluene; acetonitrile; mineral oil;

Reference yield:

: 86770-67-4
2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethanol

: 1442461-47-3
N-((1-(3,6,9,12-tetraoxapentadec-14-ynyl)-1H-1,2,3-triazol-4-yl)bis(4-fluorophenyl)methoxy)phenyl

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper(I) bromide / dichloromethane; water / 12 h / 20 °C

2.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 0 °C

2.2: 24 h / 20 °C

3.1: potassium hydrogensulfate / acetonitrile / 12 h / 20 °C

4.1: acetyl chloride / toluene / 100 °C

5.1: triethylamine; dmap / tetrahydrofuran / 12 h / 63 °C

With dmap; potassium hydrogensulfate; sodium hydride; triethylamine; acetyl chloride; copper(I) bromide; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile; mineral oil;