octadeuterodiethylene glycol ditosylate

Base Information Edit

Chemical Name:octadeuterodiethylene glycol ditosylate
CAS No.:1009630-86-7
Molecular Formula:C₁₈H₂₂O₇S₂
Molecular Weight:422.437
Hs Code.:
Mol file:1009630-86-7.mol

Synonyms:octadeuterodiethylene glycol ditosylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of octadeuterodiethylene glycol ditosylate Edit

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Technology Process of octadeuterodiethylene glycol ditosylate

There total 2 articles about octadeuterodiethylene glycol ditosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 2219-51-4
[1,1,2,2-⁽²⁾H₄]ethane-1,2-diol

: 98-59-9
p-toluenesulfonyl chloride

: 1009630-87-8
C₁₈H₁₄O₇S₂⁽²⁾H₈C₂⁽²⁾H₄O

: C₁₈H₁₄O₇S₂⁽²⁾H₈(C₂⁽²⁾H₄O)2

: 1009630-86-7
octadeuterodiethylene glycol ditosylate

Guidance literature:: [1,1,2,2-⁽²⁾H₄]ethane-1,2-diol; With iodine; at 160 - 170 ℃; for 7.5h;

p-toluenesulfonyl chloride; With potassium hydroxide; In dichloromethane; at -30 - 20 ℃; Further stages.;
DOI:10.1021/jo701979z