benzyl 2-(2-boronophenyl)ethyl ether

Base Information

Chemical Name:benzyl 2-(2-boronophenyl)ethyl ether
CAS No.:903525-00-8
Molecular Formula:C₁₅H₁₇BO₃
Molecular Weight:256.109
Hs Code.:

Synonyms:benzyl 2-(2-boronophenyl)ethyl ether

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Chemical Property of benzyl 2-(2-boronophenyl)ethyl ether

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Technology Process of benzyl 2-(2-boronophenyl)ethyl ether

There total 4 articles about benzyl 2-(2-boronophenyl)ethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1-(2-(benzyloxy)ethyl)-2-bromobenzene

: 121-43-7,63156-11-6
Trimethyl borate

: 903525-00-8
benzyl 2-(2-boronophenyl)ethyl ether

Guidance literature:: 1-(2-(benzyloxy)ethyl)-2-bromobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

Trimethyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1021/acs.jmedchem.5b01080

Reference yield: 65.0%

: 1-(2-(benzyloxy)ethyl)-2-bromobenzene

: 903525-00-8
benzyl 2-(2-boronophenyl)ethyl ether

Guidance literature:: 1-(2-(benzyloxy)ethyl)-2-bromobenzene; With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane; at -78 - 20 ℃; Inert atmosphere;

With Triisopropyl borate; In tetrahydrofuran; diethyl ether; hexane; at -78 - 20 ℃;

With water; In tetrahydrofuran; diethyl ether; hexane;

Reference yield:

: 1074-16-4
2-bromophenylethyl alcohol

: 903525-00-8
benzyl 2-(2-boronophenyl)ethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 20 - 50 °C / Inert atmosphere

1.2: 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: -78 - 20 °C

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane;
DOI:10.1021/acs.jmedchem.5b01080