C₂₁H₃₀O₃Si

Base Information

• Chemical Name: C₂₁H₃₀O₃Si
• CAS No.: 1202747-69-0
• Molecular Formula: C₂₁H₃₀O₃Si
• Molecular Weight: 358.553
• Mol file: 1202747-69-0.mol

Synonyms:C₂₁H₃₀O₃Si

Chemical Property of C₂₁H₃₀O₃Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₂₁H₃₀O₃Si

There total 2 articles about C₂₁H₃₀O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C28H36O4Si (1202748-08-0) → C21H30O3Si (1202747-69-0)

Guidance literature:

With ammonium cerium (IV) nitrate; In water; acetonitrile; at 0 ℃; Inert atmosphere;

DOI:10.1021/ja906996c

Reference yield:

tert-butylchlorodiphenylsilane (58479-61-1) → C21H30O3Si (1202747-69-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1H-imidazole; dmap / dichloromethane; N,N-dimethyl-formamide / 1.5 h / 0 - 20 °C

2: ammonium cerium (IV) nitrate; sodium hydrogencarbonate / water; acetonitrile / 0.17 h / 0 °C

With 1H-imidazole; dmap; ammonium cerium (IV) nitrate; sodium hydrogencarbonate; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1002/asia.201000882

Reference yield:

chloro-trimethyl-silane (75-77-4) + C21H30O3Si (1202747-69-0) → C27H46O3Si3 (1202747-70-3)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; for 1h; Inert atmosphere;

DOI:10.1021/ja906996c

upstream raw materials:

C₂₈H₃₆O₄Si

tert-butylchlorodiphenylsilane

Downstream raw materials:

C₂₇H₄₆O₃Si₃

C₅₅H₈₄O₉Si₂

C₅₅H₈₆O₁₁Si₂

C₂₇H₄₂O₃Si₂