hydroxy-3-dimethoxy-4,6-methyl-2-benzoate de methyle

Base Information

• Chemical Name: hydroxy-3-dimethoxy-4,6-methyl-2-benzoate de methyle
• CAS No.: 55366-04-6
• Molecular Formula: C₁₁H₁₄O₅
• Molecular Weight: 226.229
• Mol file: 55366-04-6.mol

Synonyms:hydroxy-3-dimethoxy-4,6-methyl-2-benzoate de methyle

Chemical Property of hydroxy-3-dimethoxy-4,6-methyl-2-benzoate de methyle

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of hydroxy-3-dimethoxy-4,6-methyl-2-benzoate de methyle

There total 10 articles about hydroxy-3-dimethoxy-4,6-methyl-2-benzoate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-benzoyloxy-4,6-dimethoxy-2-methyl-benzoic acid methyl ester (855366-23-3) → hydroxy-3-dimethoxy-4,6-methyl-2-benzoate de methyle (55366-04-6)

Guidance literature:

With sulfuric acid; anschliessend Behandeln mit Wasser;

DOI:10.1134/1.1333872

Reference yield:

4-[4-(3-hydroxy-4,6-dimethoxy-2-methyl-benzoyloxy)-2-methoxy-6-methyl-benzoyloxy]-2-methoxy-6-methyl-benzoic acid methyl ester → hydroxy-3-dimethoxy-4,6-methyl-2-benzoate de methyle (55366-04-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid

With sulfuric acid;

DOI:10.1134/1.1333872

Reference yield:

2-methyl-6-methoxybenzene-1,4-diol (28814-66-6) → hydroxy-3-dimethoxy-4,6-methyl-2-benzoate de methyle (55366-04-6)

Guidance literature:

Multi-step reaction with 6 steps

1: diethyl ether; HCl / und Erhitzen der Reaktionsloesung mit Wasser

2: acetone; aq. NaOH solution / unter Wasserstoff

3: methyl iodide; silver oxide; acetone

4: acetone; aqueous potassium permanganate solution

6: sulfuric acid / anschliessend Behandeln mit Wasser

With hydrogenchloride; sodium hydroxide; potassium permanganate; diethyl ether; sulfuric acid; acetone; silver(l) oxide; methyl iodide;

upstream raw materials:

diazomethane

3-hydroxy-4,6-dimethoxy-2-methyl-benzoic acid

3-benzoyloxy-4,6-dimethoxy-2-methyl-benzoic acid methyl ester

sulfuric acid

Downstream raw materials:

(benzyloxycarbonyl)-3-hydroxy-2-methoxy-4-methyl-6-benzoate de formyl-3-dihydroxy-2,4-methyl-6-phenyl

formyl-3-diisopropoxy-2,5-methoxy-4-methyl-6-benzoate de methyle

acide formyl-3-diisopropoxy-2,5-methoxy-4-methyl-6-benzoique

diisopropoxy-3,6-methoxy-2-methyl-4-benzaldehyde